(R)-3-[((S)-Cyclohexyl-methylcarbamoyl-methyl)-carbamoyl]-2,5-dimethyl-hexanoic acid

Base Information

Chemical Name:(R)-3-[((S)-Cyclohexyl-methylcarbamoyl-methyl)-carbamoyl]-2,5-dimethyl-hexanoic acid
CAS No.:205526-95-0
Molecular Formula:C₁₈H₃₂N₂O₄
Molecular Weight:340.463
Hs Code.:

Synonyms:(R)-3-[((S)-Cyclohexyl-methylcarbamoyl-methyl)-carbamoyl]-2,5-dimethyl-hexanoic acid

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Chemical Property of (R)-3-[((S)-Cyclohexyl-methylcarbamoyl-methyl)-carbamoyl]-2,5-dimethyl-hexanoic acid

Chemical Property:

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Technology Process of (R)-3-[((S)-Cyclohexyl-methylcarbamoyl-methyl)-carbamoyl]-2,5-dimethyl-hexanoic acid

There total 2 articles about (R)-3-[((S)-Cyclohexyl-methylcarbamoyl-methyl)-carbamoyl]-2,5-dimethyl-hexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 188729-01-3
(R)-3-[((S)-Cyclohexyl-methylcarbamoyl-methyl)-carbamoyl]-5-methyl-2-methylene-hexanoic acid

: 205526-95-0
(R)-3-[((S)-Cyclohexyl-methylcarbamoyl-methyl)-carbamoyl]-2,5-dimethyl-hexanoic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; Ambient temperature;
DOI:10.1021/jm970404a

Reference yield:

: 188729-00-2
2-{(R)-1-[((S)-Cyclohexyl-methylcarbamoyl-methyl)-carbamoyl]-3-methyl-butyl}-malonic acid dibenzyl ester

: 205526-95-0
(R)-3-[((S)-Cyclohexyl-methylcarbamoyl-methyl)-carbamoyl]-2,5-dimethyl-hexanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) H₂, 2.) piperidine, H₂O / 1.) 10 percent Pd/C / 1.) EtOH, RT, 4 h, 2.) EtOH, a) RT, 16 h, b) reflux, 1 h

2: H₂ / 10 percent Pd/C / methanol / Ambient temperature

With piperidine; water; hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1021/jm970404a

Reference yield:

: 205526-95-0
(R)-3-[((S)-Cyclohexyl-methylcarbamoyl-methyl)-carbamoyl]-2,5-dimethyl-hexanoic acid

: KBR 7785

Guidance literature:: Multi-step reaction with 2 steps

1: HOBT*H₂O, 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride, Et₃N / dimethylformamide / 12 h / Ambient temperature

2: 50 percent / H₂ / 10 percent Pd/C / methanol; tetrahydrofuran / Ambient temperature

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm970404a