2-[4-((E)-2-cyano-ethenesulfonyl)-phenyl]-N-[3-(2-methoxy-ethoxy)-phenyl]-isobutyramide

Base Information

Chemical Name:2-[4-((E)-2-cyano-ethenesulfonyl)-phenyl]-N-[3-(2-methoxy-ethoxy)-phenyl]-isobutyramide
CAS No.:1394819-30-7
Molecular Formula:C₂₂H₂₄N₂O₅S
Molecular Weight:428.509
Hs Code.:

Synonyms:2-[4-((E)-2-cyano-ethenesulfonyl)-phenyl]-N-[3-(2-methoxy-ethoxy)-phenyl]-isobutyramide

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Chemical Property of 2-[4-((E)-2-cyano-ethenesulfonyl)-phenyl]-N-[3-(2-methoxy-ethoxy)-phenyl]-isobutyramide

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Technology Process of 2-[4-((E)-2-cyano-ethenesulfonyl)-phenyl]-N-[3-(2-methoxy-ethoxy)-phenyl]-isobutyramide

There total 4 articles about 2-[4-((E)-2-cyano-ethenesulfonyl)-phenyl]-N-[3-(2-methoxy-ethoxy)-phenyl]-isobutyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1356089-38-7
2-[4-((E)-2-cyano-ethenesulfonyl)phenyl]-2-methylpropionic acid

: 110178-35-3
3-(2-methoxyethoxy)aniline

: 1394819-30-7
2-[4-((E)-2-cyano-ethenesulfonyl)-phenyl]-N-[3-(2-methoxy-ethoxy)-phenyl]-isobutyramide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 20 ℃;

Reference yield:

: 554-84-7
meta-nitrophenol

: 1394819-30-7
2-[4-((E)-2-cyano-ethenesulfonyl)-phenyl]-N-[3-(2-methoxy-ethoxy)-phenyl]-isobutyramide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 50 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 1551.49 Torr

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 20 °C

With hydrogen; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium 10% on activated carbon; In 1-methyl-pyrrolidin-2-one; methanol; acetonitrile;

Reference yield:

: 1-(2-methoxy-ethoxy)-3-nitro-benzene

: 1394819-30-7
2-[4-((E)-2-cyano-ethenesulfonyl)-phenyl]-N-[3-(2-methoxy-ethoxy)-phenyl]-isobutyramide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 1551.49 Torr

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 20 °C

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium 10% on activated carbon; In methanol; acetonitrile;