N-benzyloxycarbonyl-2-aminoethyl(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)(1->4)(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)(1->4)(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosiduronate

Base Information

• Chemical Name: N-benzyloxycarbonyl-2-aminoethyl(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)(1->4)(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)(1->4)(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosiduronate
• CAS No.: 1364662-69-0
• Molecular Formula: C₈₃H₁₀₁N₇O₂₉
• Molecular Weight: 1660.74

Synonyms:N-benzyloxycarbonyl-2-aminoethyl(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)(1->4)(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)(1->4)(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosiduronate

Chemical Property of N-benzyloxycarbonyl-2-aminoethyl(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)(1->4)(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)(1->4)(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosiduronate

Chemical Property:

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Technology Process of N-benzyloxycarbonyl-2-aminoethyl(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)(1->4)(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)(1->4)(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosiduronate

There total 1 articles about N-benzyloxycarbonyl-2-aminoethyl(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)(1->4)(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)(1->4)(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosiduronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

methyl (N-benzyloxycarbonyl-2-aminoethyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-α-L-idopyranoside)uronate (1364662-68-9) + O-(methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate)trichloroacetimidate (1364662-63-4) → methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-1,5-anhydro-3-O-benzyl-2-O-pivaloyl-L-xylo-hex-1-enitoluronate (1364662-70-3) + N-benzyloxycarbonyl-2-aminoethyl(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)(1->4)(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)(1->4)(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosiduronate (1364662-69-0)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1039/c2ob06607f

Reference yield: 82.0%

N-benzyloxycarbonyl-2-aminoethyl(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)(1->4)(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)(1->4)(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosiduronate (1364662-69-0) → N-benzyloxycarbonyl-2-aminoethyl(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)(1->4)(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosiduronate (1364662-71-4)

Guidance literature:

With pyridine; hydrazine hydrate; acetic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1039/c2ob06607f

upstream raw materials:

methyl (N-benzyloxycarbonyl-2-aminoethyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-α-L-idopyranoside)uronate

O-(methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate)trichloroacetimidate

Downstream raw materials:

N-benzyloxycarbonyl-2-aminoethyl(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)(methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosyluronate)(1->4)(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-α-D-glucopyranosyl)(1->4)methyl 3-O-benzyl-2-O-pivaloyl-α-L-idopyranosiduronate

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