Benzenamine, 4-(2-phenyldiazenyl)-N-(triphenylphosphoranylidene)-

Base Information

Chemical Name:Benzenamine, 4-(2-phenyldiazenyl)-N-(triphenylphosphoranylidene)-
CAS No.:33341-95-6
Molecular Formula:C₃₀H₂₄N₃P
Molecular Weight:457.514
Hs Code.:
DSSTox Substance ID:DTXSID401038387
Nikkaji Number:J3.626.302D

Synonyms:DTXSID401038387;AKOS001032120;AKOS030748574;33341-95-6;Z56762281;Benzenamine, 4-(2-phenyldiazenyl)-N-(triphenylphosphoranylidene)-;111-TRIPHENYL-N-{4-[(1E)-2-PHENYLDIAZEN-1-YL]PHENYL}-LAMBDA5-PHOSPHANIMINE

Suppliers and Price of Benzenamine, 4-(2-phenyldiazenyl)-N-(triphenylphosphoranylidene)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenamine, 4-(2-phenyldiazenyl)-N-(triphenylphosphoranylidene)-

Chemical Property:

XLogP3:8.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:457.17078478
Heavy Atom Count:34
Complexity:619

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)N=NC2=CC=C(C=C2)N=P(C3=CC=CC=C3)(C4=CC=CC=C4)C5=CC=CC=C5

Technology Process of Benzenamine, 4-(2-phenyldiazenyl)-N-(triphenylphosphoranylidene)-

There total 4 articles about Benzenamine, 4-(2-phenyldiazenyl)-N-(triphenylphosphoranylidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: C₁₂H₁₁N₅

: 603-35-0
triphenylphosphine

: 33341-95-6
4-phenylazo-N-triphenylphosphoranyliden-aniline

Guidance literature:: In toluene; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tetlet.2017.04.039

Reference yield:

: 60-09-3
aniline yellow

: 33341-95-6
4-phenylazo-N-triphenylphosphoranyliden-aniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; toluene-4-sulfonic acid / water / 0 - 20 °C

1.2: 20 °C

2.1: toluene / 2 h / 0 - 20 °C / Inert atmosphere

With toluene-4-sulfonic acid; sodium nitrite; In water; toluene; 2.1: |Staudinger Azide Reduction;
DOI:10.1016/j.tetlet.2017.04.039