3,2',6',3''-tetrakis-N-(4-methoxybenzyloxycarbonyl)-1-N-<2-(methoxybenzyloxycarbonylamino)ethoxythiocarbonyl>sisomicin

Base Information

Chemical Name:3,2',6',3''-tetrakis-N-(4-methoxybenzyloxycarbonyl)-1-N-<2-(methoxybenzyloxycarbonylamino)ethoxythiocarbonyl>sisomicin
CAS No.:79310-16-0
Molecular Formula:C₆₇H₈₂N₆O₂₃S
Molecular Weight:1371.48
Hs Code.:

Synonyms:3,2',6',3''-tetrakis-N-(4-methoxybenzyloxycarbonyl)-1-N-<2-(methoxybenzyloxycarbonylamino)ethoxythiocarbonyl>sisomicin

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Chemical Property of 3,2',6',3''-tetrakis-N-(4-methoxybenzyloxycarbonyl)-1-N-<2-(methoxybenzyloxycarbonylamino)ethoxythiocarbonyl>sisomicin

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Technology Process of 3,2',6',3''-tetrakis-N-(4-methoxybenzyloxycarbonyl)-1-N-<2-(methoxybenzyloxycarbonylamino)ethoxythiocarbonyl>sisomicin

There total 3 articles about 3,2',6',3''-tetrakis-N-(4-methoxybenzyloxycarbonyl)-1-N-<2-(methoxybenzyloxycarbonylamino)ethoxythiocarbonyl>sisomicin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 79310-21-7
1-<2-(4-methoxybenzyloxycarbonylamino)ethoxythiocarbonyl>imidazole

: 79310-15-9
3,2',6',3''-tetrakis-N-(4-methoxybenzyloxycarbonyl)sisomicin

: 79310-16-0
3,2',6',3''-tetrakis-N-(4-methoxybenzyloxycarbonyl)-1-N-<2-(methoxybenzyloxycarbonylamino)ethoxythiocarbonyl>sisomicin

Guidance literature:: With triethyloxonium fluoroborate; In dichloromethane; at 25 ℃; for 18.5h;
DOI:10.1039/P19810002186

Reference yield:

: 73352-48-4
2-(4-methoxybenzyloxycarbonylamino)ethanol

: 79310-16-0
3,2',6',3''-tetrakis-N-(4-methoxybenzyloxycarbonyl)-1-N-<2-(methoxybenzyloxycarbonylamino)ethoxythiocarbonyl>sisomicin

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / tetrahydrofuran / 2 h / Heating

2: 75 percent / triethyloxonium tetrafluoroborate / CH₂Cl₂ / 18.5 h / 25 °C

With triethyloxonium fluoroborate; In tetrahydrofuran; dichloromethane;
DOI:10.1039/P19810002186

Reference yield:

: 41840-29-3
p-methoxybenzyl-S-(4,6-dimethylpyrimidin-2-yl)-thiocarbonate

: 79310-16-0
3,2',6',3''-tetrakis-N-(4-methoxybenzyloxycarbonyl)-1-N-<2-(methoxybenzyloxycarbonylamino)ethoxythiocarbonyl>sisomicin

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / triethylamine / H₂O; dioxane / 2 h / 25 °C

2: 85 percent / tetrahydrofuran / 2 h / Heating

3: 75 percent / triethyloxonium tetrafluoroborate / CH₂Cl₂ / 18.5 h / 25 °C

With triethyloxonium fluoroborate; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
DOI:10.1039/P19810002186