Technology Process of C29H34N4O7
There total 5 articles about C29H34N4O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran;
at 20 ℃;
for 12h;
DOI:10.1002/asia.200900713
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 120 °C / Inert atmosphere
1.2: 3 h / 70 °C / Inert atmosphere
2.1: ammonia / methanol / 1 h / 20 °C
3.1: bromine; potassium hydroxide / 1,4-dioxane; water / 2.17 h / 0 - 70 °C
4.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.42 h / 0 °C
4.2: 0 - 20 °C
5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 12 h / 20 °C
With
ammonia; bromine; potassium carbonate; N-ethyl-N,N-diisopropylamine; potassium hydroxide; lithium hexamethyldisilazane;
In
tetrahydrofuran; 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;
DOI:10.1002/asia.200900713
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ammonia / methanol / 1 h / 20 °C
2.1: bromine; potassium hydroxide / 1,4-dioxane; water / 2.17 h / 0 - 70 °C
3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.42 h / 0 °C
3.2: 0 - 20 °C
4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 12 h / 20 °C
With
ammonia; bromine; N-ethyl-N,N-diisopropylamine; potassium hydroxide; lithium hexamethyldisilazane;
In
tetrahydrofuran; 1,4-dioxane; methanol; water;
DOI:10.1002/asia.200900713