{[(2-Chloro-acetyl)-(2,6-dimethyl-phenyl)-amino]-methyl}-dithiocarbamic acid isopropyl ester

Base Information

Chemical Name:{[(2-Chloro-acetyl)-(2,6-dimethyl-phenyl)-amino]-methyl}-dithiocarbamic acid isopropyl ester
CAS No.:109876-77-9
Molecular Formula:C₁₅H₂₁ClN₂OS₂
Molecular Weight:344.93
Hs Code.:

Synonyms:{[(2-Chloro-acetyl)-(2,6-dimethyl-phenyl)-amino]-methyl}-dithiocarbamic acid isopropyl ester

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Chemical Property of {[(2-Chloro-acetyl)-(2,6-dimethyl-phenyl)-amino]-methyl}-dithiocarbamic acid isopropyl ester

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Technology Process of {[(2-Chloro-acetyl)-(2,6-dimethyl-phenyl)-amino]-methyl}-dithiocarbamic acid isopropyl ester

There total 3 articles about {[(2-Chloro-acetyl)-(2,6-dimethyl-phenyl)-amino]-methyl}-dithiocarbamic acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 81140-63-8
N-(2,6-Dimethylphenyl),N-isothiocyanatomethyl chloroacetamide

: 75-33-2
2-propanethiol

: 109876-77-9
{[(2-Chloro-acetyl)-(2,6-dimethyl-phenyl)-amino]-methyl}-dithiocarbamic acid isopropyl ester

Guidance literature:: In chloroform; for 0.5h; Ambient temperature;
DOI:10.1055/s-1986-31789

Reference yield:

: 61706-54-5
N-(chloromethyl)-N-(2,6-dimethylphenyl)-α-chloroacetamide

: 109876-77-9
{[(2-Chloro-acetyl)-(2,6-dimethyl-phenyl)-amino]-methyl}-dithiocarbamic acid isopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / acetone / 1 h / 20 °C

2: 75 percent / butan-2-one / 3.5 h / 80 °C

3: 94 percent / CHCl₃ / 0.5 h / Ambient temperature

In chloroform; acetone; butanone;
DOI:10.1055/s-1986-31789

Reference yield:

: 81140-62-7
2-Chloro-N-(2,6-dimethyl-phenyl)-N-thiocyanatomethyl-acetamide

: 109876-77-9
{[(2-Chloro-acetyl)-(2,6-dimethyl-phenyl)-amino]-methyl}-dithiocarbamic acid isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / butan-2-one / 3.5 h / 80 °C

2: 94 percent / CHCl₃ / 0.5 h / Ambient temperature

In chloroform; butanone;
DOI:10.1055/s-1986-31789