2-(2,6-Dimethylphenyl)-5-isopropyl-6-oxo-4,5,6,7-tetrahydro-1,3,5-thiadiazepine

Base Information

Chemical Name:2-(2,6-Dimethylphenyl)-5-isopropyl-6-oxo-4,5,6,7-tetrahydro-1,3,5-thiadiazepine
CAS No.:109876-68-8
Molecular Formula:C₁₅H₂₀N₂OS₂
Molecular Weight:308.469
Hs Code.:

Synonyms:2-(2,6-Dimethylphenyl)-5-isopropyl-6-oxo-4,5,6,7-tetrahydro-1,3,5-thiadiazepine

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Chemical Property of 2-(2,6-Dimethylphenyl)-5-isopropyl-6-oxo-4,5,6,7-tetrahydro-1,3,5-thiadiazepine

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Technology Process of 2-(2,6-Dimethylphenyl)-5-isopropyl-6-oxo-4,5,6,7-tetrahydro-1,3,5-thiadiazepine

There total 4 articles about 2-(2,6-Dimethylphenyl)-5-isopropyl-6-oxo-4,5,6,7-tetrahydro-1,3,5-thiadiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 109876-77-9
{[(2-Chloro-acetyl)-(2,6-dimethyl-phenyl)-amino]-methyl}-dithiocarbamic acid isopropyl ester

: 109876-68-8
2-(2,6-Dimethylphenyl)-5-isopropyl-6-oxo-4,5,6,7-tetrahydro-1,3,5-thiadiazepine

Guidance literature:: With potassium hydroxide; In methanol; at 30 ℃; for 4h;
DOI:10.1055/s-1986-31789

Reference yield:

: 61706-54-5
N-(chloromethyl)-N-(2,6-dimethylphenyl)-α-chloroacetamide

: 109876-68-8
2-(2,6-Dimethylphenyl)-5-isopropyl-6-oxo-4,5,6,7-tetrahydro-1,3,5-thiadiazepine

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / acetone / 1 h / 20 °C

2: 75 percent / butan-2-one / 3.5 h / 80 °C

3: 94 percent / CHCl₃ / 0.5 h / Ambient temperature

4: 90 percent / KOH / methanol / 4 h / 30 °C

With potassium hydroxide; In methanol; chloroform; acetone; butanone;
DOI:10.1055/s-1986-31789

Reference yield:

: 81140-63-8
N-(2,6-Dimethylphenyl),N-isothiocyanatomethyl chloroacetamide

: 109876-68-8
2-(2,6-Dimethylphenyl)-5-isopropyl-6-oxo-4,5,6,7-tetrahydro-1,3,5-thiadiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / CHCl₃ / 0.5 h / Ambient temperature

2: 90 percent / KOH / methanol / 4 h / 30 °C

With potassium hydroxide; In methanol; chloroform;
DOI:10.1055/s-1986-31789