3-O-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl]tigogenin

Base Information

• Chemical Name: 3-O-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl]tigogenin
• CAS No.: 1352548-84-5
• Molecular Formula: C₈₈H₉₂O₂₀
• Molecular Weight: 1469.69

Synonyms:3-O-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl]tigogenin

Chemical Property of 3-O-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl]tigogenin

Chemical Property:

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Technology Process of 3-O-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl]tigogenin

There total 1 articles about 3-O-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl]tigogenin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

tigogenin (77-60-1) + 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl trichloroacetimidate (773145-61-2) → 3-O-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl]tigogenin (1352548-84-5)

Guidance literature:

tigogenin; 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl trichloroacetimidate; In dichloromethane; for 1h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 3h; Inert atmosphere;

DOI:10.1016/j.bmcl.2011.10.015

Reference yield: 85.0%

3-O-[2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl]tigogenin (1352548-84-5) → tiqueside (99759-19-0)

Guidance literature:

With methanol; sodium methylate; In dichloromethane; at 20 ℃; for 1h; pH=10;

DOI:10.1016/j.bmcl.2011.10.015

upstream raw materials:

tigogenin

2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl trichloroacetimidate

Downstream raw materials:

tiqueside

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