5-(4,6-bis(3-methoxyphenylamino)-1,3,5-triazin-2-ylamino)picolinonitrile

Base Information

• Chemical Name: 5-(4,6-bis(3-methoxyphenylamino)-1,3,5-triazin-2-ylamino)picolinonitrile
• CAS No.: 1393551-03-5
• Molecular Formula: C₂₃H₂₀N₈O₂
• Molecular Weight: 440.464

Synonyms:5-(4,6-bis(3-methoxyphenylamino)-1,3,5-triazin-2-ylamino)picolinonitrile

Chemical Property of 5-(4,6-bis(3-methoxyphenylamino)-1,3,5-triazin-2-ylamino)picolinonitrile

Chemical Property:

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Technology Process of 5-(4,6-bis(3-methoxyphenylamino)-1,3,5-triazin-2-ylamino)picolinonitrile

There total 2 articles about 5-(4,6-bis(3-methoxyphenylamino)-1,3,5-triazin-2-ylamino)picolinonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]pyridine-2-carbonitrile (1393550-77-0) + m-Anisidine (536-90-3,918666-97-4) → 5-(4,6-bis(3-methoxyphenylamino)-1,3,5-triazin-2-ylamino)picolinonitrile (1393551-03-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 5h;

DOI:10.1016/j.bmcl.2012.05.111

Reference yield:

5-amino-2-cyanopyridine (55338-73-3) → 5-(4,6-bis(3-methoxyphenylamino)-1,3,5-triazin-2-ylamino)picolinonitrile (1393551-03-5)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone / 6 h / 0 - 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C

With potassium carbonate; In N,N-dimethyl-formamide; acetone;

DOI:10.1016/j.bmcl.2012.05.111

Reference yield: 85.0%

5-(4,6-bis(3-methoxyphenylamino)-1,3,5-triazin-2-ylamino)picolinonitrile (1393551-03-5) → 5-(4,6-bis(3-methoxyphenylamino)-1,3,5-triazin-2-ylamino)picolinonitrile hydrochloride

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;

DOI:10.1016/j.bmcl.2012.05.111

upstream raw materials:

5-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]pyridine-2-carbonitrile

m-Anisidine

5-amino-2-cyanopyridine

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