N-[(1S,2R,3S,4R)-3-(4-methoxybenzoylamino)-4,7,7-trimethylbicyclo[2.2.1]hept-2-yl]pyrazine-2-carboxamide

Base Information

Chemical Name:N-[(1S,2R,3S,4R)-3-(4-methoxybenzoylamino)-4,7,7-trimethylbicyclo[2.2.1]hept-2-yl]pyrazine-2-carboxamide
CAS No.:1394897-81-4
Molecular Formula:C₂₃H₂₈N₄O₃
Molecular Weight:408.5
Hs Code.:

Synonyms:N-[(1S,2R,3S,4R)-3-(4-methoxybenzoylamino)-4,7,7-trimethylbicyclo[2.2.1]hept-2-yl]pyrazine-2-carboxamide

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Chemical Property of N-[(1S,2R,3S,4R)-3-(4-methoxybenzoylamino)-4,7,7-trimethylbicyclo[2.2.1]hept-2-yl]pyrazine-2-carboxamide

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Technology Process of N-[(1S,2R,3S,4R)-3-(4-methoxybenzoylamino)-4,7,7-trimethylbicyclo[2.2.1]hept-2-yl]pyrazine-2-carboxamide

There total 4 articles about N-[(1S,2R,3S,4R)-3-(4-methoxybenzoylamino)-4,7,7-trimethylbicyclo[2.2.1]hept-2-yl]pyrazine-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1394897-79-0
C₂₃H₂₆N₄O₂

: 1394897-81-4
N-[(1S,2R,3S,4R)-3-(4-methoxybenzoylamino)-4,7,7-trimethylbicyclo[2.2.1]hept-2-yl]pyrazine-2-carboxamide

Guidance literature:: With water; for 730.5h; Storing conditions; Neat (no solvent);
DOI:10.1016/j.tetasy.2012.06.016

Reference yield:

: 74617-55-3
pyrazine-2-carboximidic acid methyl ester

: 1394897-81-4
N-[(1S,2R,3S,4R)-3-(4-methoxybenzoylamino)-4,7,7-trimethylbicyclo[2.2.1]hept-2-yl]pyrazine-2-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; triethylamine / methanol / 12 h / 40 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 3 h / 0 - 25 °C / Inert atmosphere

3.1: water / 730.5 h / Storing conditions; Neat (no solvent)

With water; acetic acid; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetasy.2012.06.016

Reference yield:

: 19847-12-2
2-pyrazine carbonitrile

: 1394897-81-4
N-[(1S,2R,3S,4R)-3-(4-methoxybenzoylamino)-4,7,7-trimethylbicyclo[2.2.1]hept-2-yl]pyrazine-2-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium / 25 °C

2.1: acetic acid; triethylamine / methanol / 12 h / 40 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.2: 3 h / 0 - 25 °C / Inert atmosphere

4.1: water / 730.5 h / Storing conditions; Neat (no solvent)

With water; sodium; acetic acid; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetasy.2012.06.016