2-methyl-1,3-phenylene bis{4[-4-(undec-10-enyloxy)phenoxycarbonyl]benzoate}

Base Information

Chemical Name:2-methyl-1,3-phenylene bis{4[-4-(undec-10-enyloxy)phenoxycarbonyl]benzoate}
CAS No.:1185417-91-7
Molecular Formula:C₅₇H₆₄O₁₀
Molecular Weight:909.129
Hs Code.:

Synonyms:2-methyl-1,3-phenylene bis{4[-4-(undec-10-enyloxy)phenoxycarbonyl]benzoate}

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Chemical Property of 2-methyl-1,3-phenylene bis{4[-4-(undec-10-enyloxy)phenoxycarbonyl]benzoate}

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Technology Process of 2-methyl-1,3-phenylene bis{4[-4-(undec-10-enyloxy)phenoxycarbonyl]benzoate}

There total 3 articles about 2-methyl-1,3-phenylene bis{4[-4-(undec-10-enyloxy)phenoxycarbonyl]benzoate} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 576-26-1,25134-01-4
2.6-dimethylphenol

: 1185417-88-2
4-[4-(undec-10-enyloxy)phenoxycarbonyl]benzoic acid

: 1185417-91-7
2-methyl-1,3-phenylene bis{4[-4-(undec-10-enyloxy)phenoxycarbonyl]benzoate}

Guidance literature:: 2.6-dimethylphenol; 4-[4-(undec-10-enyloxy)phenoxycarbonyl]benzoic acid; With dmap; In dichloromethane; for 0.166667h;

With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1039/b907536d

Reference yield:

: 117721-44-5
p-hydroxyphenyl undec-10-en-1-yl ether

: 1185417-91-7
2-methyl-1,3-phenylene bis{4[-4-(undec-10-enyloxy)phenoxycarbonyl]benzoate}

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap / dichloromethane / 0.17 h

1.2: 12 h / 20 °C

2.1: sodium chlorite; sodium dihydrogen phosphate monohydrate; recorcinol / water; tert-butyl alcohol / 20 °C

2.2: pH 2

3.1: dmap / dichloromethane / 0.17 h

3.2: 12 h / 20 °C

With dmap; sodium chlorite; sodium dihydrogen phosphate monohydrate; recorcinol; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/b907536d

Reference yield:

: 619-66-9
4-Carboxybenzaldehyde

: 1185417-91-7
2-methyl-1,3-phenylene bis{4[-4-(undec-10-enyloxy)phenoxycarbonyl]benzoate}

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap / dichloromethane / 0.17 h

1.2: 12 h / 20 °C

2.1: sodium chlorite; sodium dihydrogen phosphate monohydrate; recorcinol / water; tert-butyl alcohol / 20 °C

2.2: pH 2

With dmap; sodium chlorite; sodium dihydrogen phosphate monohydrate; recorcinol; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/b907536d