4-[(Undec-10-en-1-yl)oxy]phenol

Base Information

• Chemical Name: 4-[(Undec-10-en-1-yl)oxy]phenol
• CAS No.: 117721-44-5
• Molecular Formula: C17H26O2
• Molecular Weight: 262.392
• DSSTox Substance ID: DTXSID30592807
• Wikidata: Q82487123
• Mol file: 117721-44-5.mol

Synonyms:117721-44-5;4-[(Undec-10-en-1-yl)oxy]phenol;4-(10-undecenoxy)phenol;p-(10-undecenyl)oxyphenol;SCHEMBL2849938;DTXSID30592807;PYOLOAGQFRDAPH-UHFFFAOYSA-N;4-(UNDEC-10-EN-1-YLOXY)PHENOL

Chemical Property of 4-[(Undec-10-en-1-yl)oxy]phenol

Chemical Property:

• XLogP3: 6.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 11
• Exact Mass: 262.193280068
• Heavy Atom Count: 19
• Complexity: 207

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CCCCCCCCCCOC1=CC=C(C=C1)O

Technology Process of 4-[(Undec-10-en-1-yl)oxy]phenol

There total 4 articles about 4-[(Undec-10-en-1-yl)oxy]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

4-(undec-10-enoxy)anisole (121269-09-8) → p-hydroxyphenyl undec-10-en-1-yl ether (117721-44-5)

Guidance literature:

With sodium thioethylate; In N,N-dimethyl-formamide; at 120 ℃; for 24h;

DOI:10.3987/com-02-9437

Reference yield: 68.0%

1-undecen-11-ylbromide (7766-50-9) + hydroquinone (123-31-9,8027-02-9) → p-hydroxyphenyl undec-10-en-1-yl ether (117721-44-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 48h;

DOI:10.1021/ja077392v

Reference yield:

1-undecen-11-ylbromide (7766-50-9) → p-hydroxyphenyl undec-10-en-1-yl ether (117721-44-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 71 percent / potassium carbonate; potassium iodide / dimethylformamide / 24 h / 160 °C

2: 79 percent / sodium ethanethiolate / dimethylformamide / 24 h / 120 °C

With potassium carbonate; potassium iodide; sodium thioethylate; In N,N-dimethyl-formamide;

DOI:10.3987/com-02-9437

upstream raw materials:

4-(undec-10-enoxy)anisole

1-undecen-11-ylbromide

4-methoxy-phenol

hydroquinone

Downstream raw materials:

(S_C)-5-ethyl-3-(2-methylbutoxy)-7-(4-undec-10-enoxyphenoxycarbonyl)-5H-dibenzophosphole 5-oxide

(S_C,S_P)-5-ethyl-3-(2-methylbutoxy)-7-(4-undec-10-enoxyphenoxycarbonyl)-5H-dibenzophosphole

4-(undec-10-enyloxy)phenyl 4-formylbenzoate

4-[4-(undec-10-enyloxy)phenoxycarbonyl]benzoic acid