4-acetyl-2-allylphenyl trifluoromethanesulfonate

Base Information

Chemical Name:4-acetyl-2-allylphenyl trifluoromethanesulfonate
CAS No.:1229611-30-6
Molecular Formula:C₁₂H₁₁F₃O₄S
Molecular Weight:308.278
Hs Code.:

Synonyms:4-acetyl-2-allylphenyl trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-acetyl-2-allylphenyl trifluoromethanesulfonate

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Technology Process of 4-acetyl-2-allylphenyl trifluoromethanesulfonate

There total 1 articles about 4-acetyl-2-allylphenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1132-05-4
3-allyl-4-hydroxyacetophenone

: 1229611-30-6
4-acetyl-2-allylphenyl trifluoromethanesulfonate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1021/acs.joc.7b00200

Reference yield: 99.0%

: 1229611-30-6
4-acetyl-2-allylphenyl trifluoromethanesulfonate

: 1229611-31-7
(E)-4-acetyl-2-(1-propenyl)phenyl triflate

Guidance literature:: With tri-tert-butyl phosphine; isobutyryl chloride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; at 80 ℃; for 20h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ja9108424

Reference yield: 91.0%

: 1229611-30-6
4-acetyl-2-allylphenyl trifluoromethanesulfonate

: 126726-62-3
2-isopropenyl-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 1-(3-allyl-4-(prop-1-en-2-yl)phenyl)ethan-1-one

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; water; at 120 ℃; for 18h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.7b00200