Technology Process of Ketone, inden-6-yl methyl (7CI)
There total 4 articles about Ketone, inden-6-yl methyl (7CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Hoveyda-Grubbs catalyst second generation;
In
dichloromethane;
at 40 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/acs.joc.7b00200
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 0 °C / Inert atmosphere
2: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 18 h / 120 °C / Schlenk technique; Inert atmosphere
3: Hoveyda-Grubbs catalyst second generation / dichloromethane / 1 h / 40 °C / Inert atmosphere
With
pyridine; tetrakis(triphenylphosphine) palladium(0); Hoveyda-Grubbs catalyst second generation; potassium carbonate;
In
1,4-dioxane; dichloromethane; water;
2: |Suzuki Coupling;
DOI:10.1021/acs.joc.7b00200
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 18 h / 120 °C / Schlenk technique; Inert atmosphere
2: Hoveyda-Grubbs catalyst second generation / dichloromethane / 1 h / 40 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); Hoveyda-Grubbs catalyst second generation; potassium carbonate;
In
1,4-dioxane; dichloromethane; water;
1: |Suzuki Coupling;
DOI:10.1021/acs.joc.7b00200
