C₄₂H₃₈O₁₀

Base Information

Chemical Name:C₄₂H₃₈O₁₀
CAS No.:1053254-94-6
Molecular Formula:C₄₂H₃₈O₁₀
Molecular Weight:702.758
Hs Code.:

C<sub>42</sub>H<sub>38</sub>O<sub>10</sub>

Synonyms:C₄₂H₃₈O₁₀

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Chemical Property of C₄₂H₃₈O₁₀

Chemical Property:

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Technology Process of C₄₂H₃₈O₁₀

There total 13 articles about C₄₂H₃₈O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 98-88-4
benzoyl chloride

: C₃₅H₃₄O₉

: 1053254-94-6
C₄₂H₃₈O₁₀

Guidance literature:: With pyridine;
DOI:10.1021/jo00088a003

Reference yield:

: 642-38-6
quebrachitol

: 1053254-94-6
C₄₂H₃₈O₁₀

Guidance literature:: Multi-step reaction with 13 steps

1: 81 percent / camphorsulfonic acid / dimethylformamide / 5 h / 70 °C

2: 92 percent / TEA / CH₂Cl₂ / 2 h / 0 °C

3: 82 percent / BBr₃ / CH₂Cl₂ / Ambient temperature

4: camphorsulfonic acid / dimethylformamide / 5 h / 70 °C

5: 99 percent / NaH / dimethylformamide / 0 °C

6: 82 percent / LiAlH₄ / tetrahydrofuran / 5 h / Ambient temperature

7: 1.) (COCl)2, DMSO, 2.) diisopropylamine / 1.) CH₂Cl₂, 2.) -78 deg C to -10 deg C

8: LiBH₄ / tetrahydrofuran / -78 °C

9: 92 percent / NaH / dimethylformamide / 7 h

10: 73 percent / AcCl / CH₂Cl₂; methanol / 0.25 h / Ambient temperature

11: pyridine / Ambient temperature

12: 84 percent / conc. HCl / CH₂Cl₂; methanol / 9 h / Ambient temperature

13: 95 percent / pyridine

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; lithium borohydride; oxalyl dichloride; TEA; camphor-10-sulfonic acid; boron tribromide; sodium hydride; dimethyl sulfoxide; diisopropylamine; acetyl chloride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00088a003

Reference yield:

: 58769-23-6
1L-3,4,:5,6-di-O-isopropylidene-2-O-methyl-chiro-inositol

: 1053254-94-6
C₄₂H₃₈O₁₀

Guidance literature:: Multi-step reaction with 12 steps

1: 92 percent / TEA / CH₂Cl₂ / 2 h / 0 °C

2: 82 percent / BBr₃ / CH₂Cl₂ / Ambient temperature

3: camphorsulfonic acid / dimethylformamide / 5 h / 70 °C

4: 99 percent / NaH / dimethylformamide / 0 °C

5: 82 percent / LiAlH₄ / tetrahydrofuran / 5 h / Ambient temperature

6: 1.) (COCl)2, DMSO, 2.) diisopropylamine / 1.) CH₂Cl₂, 2.) -78 deg C to -10 deg C

7: LiBH₄ / tetrahydrofuran / -78 °C

8: 92 percent / NaH / dimethylformamide / 7 h

9: 73 percent / AcCl / CH₂Cl₂; methanol / 0.25 h / Ambient temperature

10: pyridine / Ambient temperature

11: 84 percent / conc. HCl / CH₂Cl₂; methanol / 9 h / Ambient temperature

12: 95 percent / pyridine

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; lithium borohydride; oxalyl dichloride; TEA; camphor-10-sulfonic acid; boron tribromide; sodium hydride; dimethyl sulfoxide; diisopropylamine; acetyl chloride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00088a003