2-(2-{4-[2-(2-tosyloxyethoxy)ethoxymethyl]benzyloxy}ethoxy)ethyl toluene-4-sulfonate

Base Information

Chemical Name:2-(2-{4-[2-(2-tosyloxyethoxy)ethoxymethyl]benzyloxy}ethoxy)ethyl toluene-4-sulfonate
CAS No.:881890-43-3
Molecular Formula:C₃₀H₃₈O₁₀S₂
Molecular Weight:622.758
Hs Code.:

Synonyms:2-(2-{4-[2-(2-tosyloxyethoxy)ethoxymethyl]benzyloxy}ethoxy)ethyl toluene-4-sulfonate

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Chemical Property of 2-(2-{4-[2-(2-tosyloxyethoxy)ethoxymethyl]benzyloxy}ethoxy)ethyl toluene-4-sulfonate

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Technology Process of 2-(2-{4-[2-(2-tosyloxyethoxy)ethoxymethyl]benzyloxy}ethoxy)ethyl toluene-4-sulfonate

There total 1 articles about 2-(2-{4-[2-(2-tosyloxyethoxy)ethoxymethyl]benzyloxy}ethoxy)ethyl toluene-4-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 98-59-9
p-toluenesulfonyl chloride

: 183151-57-7
2-(2-{4-[2-(2-hydroxyethoxy)ethoxymethyl]benzyloxy}ethoxy)ethanol

: 881890-43-3
2-(2-{4-[2-(2-tosyloxyethoxy)ethoxymethyl]benzyloxy}ethoxy)ethyl toluene-4-sulfonate

Guidance literature:: With sodium hydroxide; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1002/ejoc.200500421

Reference yield: 76.0%

: 881890-42-2
2,6-dimethyl-4-tritylphenol

: 881890-43-3
2-(2-{4-[2-(2-tosyloxyethoxy)ethoxymethyl]benzyloxy}ethoxy)ethyl toluene-4-sulfonate

: 881890-44-4
2-[2-(4-{2-[2-(2,6-dimethyl-4-tritylphenoxy)ethoxy]ethoxymethyl}benzyloxy)ethoxy]ethyl toluene-4-sulfonate

Guidance literature:: With sodium ethanolate; In acetonitrile; for 4h; Heating;
DOI:10.1002/ejoc.200500421

Reference yield:

: 881890-43-3
2-(2-{4-[2-(2-tosyloxyethoxy)ethoxymethyl]benzyloxy}ethoxy)ethyl toluene-4-sulfonate

: 881890-45-5
4-{2-[2-(4-{2-[2-(2,6-dimethyl-4-tritylphenoxy)ethoxy]ethoxymethyl}benzyloxy)ethoxy]ethoxy}but-2-yn-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / NaOEt / acetonitrile / 4 h / Heating

2: 65 percent / NaOEt / dimethylsulfoxide / 90 °C

With sodium ethanolate; In dimethyl sulfoxide; acetonitrile;
DOI:10.1002/ejoc.200500421