2,6-dimethoxy-4-(5-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-3-yl)phenol

Base Information

Chemical Name:2,6-dimethoxy-4-(5-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-3-yl)phenol
CAS No.:1227741-03-8
Molecular Formula:C₂₀H₂₃NO₇
Molecular Weight:389.405
Hs Code.:

Synonyms:2,6-dimethoxy-4-(5-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-3-yl)phenol

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Chemical Property of 2,6-dimethoxy-4-(5-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-3-yl)phenol

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Technology Process of 2,6-dimethoxy-4-(5-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-3-yl)phenol

There total 5 articles about 2,6-dimethoxy-4-(5-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-3-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1272644-64-0
3-(4-(tert-butyldimethylsilyloxy)-3,5-dimethoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazole

: 1227741-03-8
2,6-dimethoxy-4-(5-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-3-yl)phenol

Guidance literature:: 3-(4-(tert-butyldimethylsilyloxy)-3,5-dimethoxyphenyl)-5-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazole; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;

With water; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.ejmech.2010.12.004

Reference yield:

: 1246651-17-1
4-(tert-butyl-dimethyl-silyloxy)-3,5-dimethoxybenzaldehyde oxime

: 1227741-03-8
2,6-dimethoxy-4-(5-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-3-yl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hypochlorite; triethylamine / dichloromethane; water / 25 h / 0 - 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

2.2: 20 °C

With sodium hypochlorite; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.ejmech.2010.12.004

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 1227741-03-8
2,6-dimethoxy-4-(5-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-3-yl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 5 h / 20 °C

2.1: sodium hypochlorite; triethylamine / dichloromethane; water / 25 h / 0 - 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

3.2: 20 °C

With sodium hypochlorite; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; water; mineral oil;
DOI:10.1016/j.ejmech.2010.12.004