Technology Process of C18H17NO7
There total 3 articles about C18H17NO7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: nitric acid; acetic anhydride; acetic acid / dichloromethane; water / 1.18 h / 0 - 20 °C
2.1: thionyl chloride / 24 h / Heating / reflux
3.1: potassium carbonate; sodium iodide / 1,4-dioxane; N,N-dimethyl-formamide; toluene / 72 h
4.1: N,N-dimethyl-formamide dimethyl acetal / N,N-dimethyl-formamide / 18 h / 125 °C
4.2: 0.5 h
With
thionyl chloride; nitric acid; acetic anhydride; potassium carbonate; acetic acid; N,N-dimethyl-formamide dimethyl acetal; sodium iodide;
In
1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate; sodium iodide / 1,4-dioxane; N,N-dimethyl-formamide; toluene / 72 h
2.1: N,N-dimethyl-formamide dimethyl acetal / N,N-dimethyl-formamide / 18 h / 125 °C
2.2: 0.5 h
With
potassium carbonate; N,N-dimethyl-formamide dimethyl acetal; sodium iodide;
In
1,4-dioxane; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: thionyl chloride / 24 h / Heating / reflux
2.1: potassium carbonate; sodium iodide / 1,4-dioxane; N,N-dimethyl-formamide; toluene / 72 h
3.1: N,N-dimethyl-formamide dimethyl acetal / N,N-dimethyl-formamide / 18 h / 125 °C
3.2: 0.5 h
With
thionyl chloride; potassium carbonate; N,N-dimethyl-formamide dimethyl acetal; sodium iodide;
In
1,4-dioxane; N,N-dimethyl-formamide; toluene;
