3-<(p-ethoxyethoxyethoxyphenyl)(4-phenyl-3,5-dioxacyclohexyl)methyl>-1,5,8,11-tetraoxacyclotridecane

Base Information

Chemical Name:3-<(p-ethoxyethoxyethoxyphenyl)(4-phenyl-3,5-dioxacyclohexyl)methyl>-1,5,8,11-tetraoxacyclotridecane
CAS No.:126750-16-1
Molecular Formula:C₃₂H₄₆O₉
Molecular Weight:574.712
Hs Code.:

Synonyms:3-<(p-ethoxyethoxyethoxyphenyl)(4-phenyl-3,5-dioxacyclohexyl)methyl>-1,5,8,11-tetraoxacyclotridecane

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Chemical Property of 3-<(p-ethoxyethoxyethoxyphenyl)(4-phenyl-3,5-dioxacyclohexyl)methyl>-1,5,8,11-tetraoxacyclotridecane

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Technology Process of 3-<(p-ethoxyethoxyethoxyphenyl)(4-phenyl-3,5-dioxacyclohexyl)methyl>-1,5,8,11-tetraoxacyclotridecane

There total 7 articles about 3-<(p-ethoxyethoxyethoxyphenyl)(4-phenyl-3,5-dioxacyclohexyl)methyl>-1,5,8,11-tetraoxacyclotridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126750-14-9
2-phenyl-5-<1-(p-ethoxyethoxyethoxyphenyl)-2,2-di(hydroxymethyl)ethyl>-1,3-dioxane

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 126750-16-1
3-<(p-ethoxyethoxyethoxyphenyl)(4-phenyl-3,5-dioxacyclohexyl)methyl>-1,5,8,11-tetraoxacyclotridecane

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) dioxane, 70 deg C, 1 h, 2.) 80 deg C, 10 h;

Reference yield:

: 126750-26-3
1-ethoxy-2-(2-(2-iodoethoxy)ethoxy)ethane

: 126750-16-1
3-<(p-ethoxyethoxyethoxyphenyl)(4-phenyl-3,5-dioxacyclohexyl)methyl>-1,5,8,11-tetraoxacyclotridecane

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) sodium hydroxide / 1.) butyl alcolhol, reflux, 1 h, 2.) reflux, 12 h

2: 78 percent / piperidine / benzene / 12 h / Heating

3: 63 percent / activated zinc, iodine / tetrahydrofuran / 5 h / 50 °C

4: 85 percent / lithium aluminum hydride / diethyl ether / 1.) reflux, 2 h, 2.) room temp., 24 h

5: 70 percent / conc. HCl / dimethylformamide / 7 h / 30 °C

6: 1.) NaH / 1.) dioxane, 70 deg C, 1 h, 2.) 80 deg C, 10 h

With piperidine; hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; iodine; sodium hydride; zinc; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; benzene;

Reference yield:

: 117420-31-2
4-(2-(2-ethoxyethoxy)ethoxy)benzaldehyde

: 126750-16-1
3-<(p-ethoxyethoxyethoxyphenyl)(4-phenyl-3,5-dioxacyclohexyl)methyl>-1,5,8,11-tetraoxacyclotridecane

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / piperidine / benzene / 12 h / Heating

2: 63 percent / activated zinc, iodine / tetrahydrofuran / 5 h / 50 °C

3: 85 percent / lithium aluminum hydride / diethyl ether / 1.) reflux, 2 h, 2.) room temp., 24 h

4: 70 percent / conc. HCl / dimethylformamide / 7 h / 30 °C

5: 1.) NaH / 1.) dioxane, 70 deg C, 1 h, 2.) 80 deg C, 10 h

With piperidine; hydrogenchloride; lithium aluminium tetrahydride; iodine; sodium hydride; zinc; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; benzene;