ethyl 3--4-(3-furyl)-4-oxobutyrate

Base Information

Chemical Name:ethyl 3--4-(3-furyl)-4-oxobutyrate
CAS No.:88352-61-8
Molecular Formula:C₁₇H₁₆ClNO₅
Molecular Weight:349.771
Hs Code.:

ethyl 3-<N-(4-chlorobenzoyl)amino>-4-(3-furyl)-4-oxobutyrate

Synonyms:ethyl 3--4-(3-furyl)-4-oxobutyrate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 3--4-(3-furyl)-4-oxobutyrate

Chemical Property:

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Technology Process of ethyl 3--4-(3-furyl)-4-oxobutyrate

There total 3 articles about ethyl 3--4-(3-furyl)-4-oxobutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.5%

: 88352-61-8
ethyl 3--4-(3-furyl)-4-oxobutyrate

: 10025-87-3,12599-09-6,63736-95-8,39380-77-3
trichlorophosphate

Guidance literature:

Reference yield: 77.3%

: 105-36-2
ethyl bromoacetate

: 88352-91-4
N-<(4-chlorobenzoyl)amino>methyl 3-furyl ketone

: 88352-61-8
ethyl 3--4-(3-furyl)-4-oxobutyrate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; paraffin; 1.) -50 - -40 deg C, 20 min, 2.) -40 to 10 deg C, 30 min;
DOI:10.1021/jm00401a021

Reference yield:

: 88352-90-3
aminomethyl 3-furyl ketone hydrochloride

: 88352-61-8
ethyl 3--4-(3-furyl)-4-oxobutyrate

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / H₂O; ethyl acetate / Ambient temperature

2: 77 percent / NaH / paraffin; dimethylformamide / 1.) -50 - -40 deg C, 20 min, 2.) -40 to 10 deg C, 30 min

With sodium hydride; sodium hydrogencarbonate; In water; ethyl acetate; N,N-dimethyl-formamide; paraffin;
DOI:10.1021/jm00401a021