2-benzoyl-2-propaneseleninic acid

Base Information

• Chemical Name: 2-benzoyl-2-propaneseleninic acid
• CAS No.: 81360-92-1
• Molecular Formula: C₁₀H₁₂O₃Se
• Molecular Weight: 259.163
• Mol file: 81360-92-1.mol

Synonyms:2-benzoyl-2-propaneseleninic acid

Chemical Property of 2-benzoyl-2-propaneseleninic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-benzoyl-2-propaneseleninic acid

There total 6 articles about 2-benzoyl-2-propaneseleninic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

bis-(2-benzoyl-2-propyl) diselenide (81360-90-9) → 2-benzoyl-2-propaneseleninic acid (81360-92-1)

Guidance literature:

With ozone; In diethyl ether; water; at -78 ℃;

DOI:10.1016/S0040-4020(01)96716-X

Reference yield:

2,2'-diseleno-bis(1-phenyl-2-methyl-1-propanone)-Se-oxide (81360-89-6) → 2-methyl-1-phenylprop-2-en-1-one (769-60-8) + 2-benzoyl-2-propaneseleninic acid (81360-92-1) + bis-(2-benzoyl-2-propyl) diselenide (81360-90-9) + C20H22O2Se3 (104722-74-9)

Guidance literature:

In dichloromethane-d2; at -50 - 25 ℃; for 0.0833333h; Title compound not separated from byproducts;

DOI:10.1016/S0040-4020(01)96716-X

Reference yield:

2,2'-diseleno-bis(1-phenyl-2-methyl-1-propanone)-Se-oxide (81360-89-6) → 2-benzoyl-2-propaneseleninic acid (81360-92-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 22 percent Spectr_. / CD₂Cl₂ / 0.08 h / -50 - 25 °C

2: 98 percent / O₃ / H₂O; diethyl ether / -78 °C

With ozone; In diethyl ether; dichloromethane-d2; water;

DOI:10.1016/S0040-4020(01)96716-X

upstream raw materials:

2,2'-diseleno-bis(1-phenyl-2-methyl-1-propanone)-Se-oxide

bis-(2-benzoyl-2-propyl) diselenide

1-phenyl-2-(chloroseleno)-2-methylpropanone

bis-2-benzoyl-2-propyl selenide

Downstream raw materials:

2-methyl-1-phenylprop-2-en-1-one

2,2'-diseleno-bis(1-phenyl-2-methyl-1-propanone)-Se-oxide

1-phenyl-2-(chloroseleno)-2-methylpropanone

N,N-dimethyl 2-benzoyl-2-propane selenenamide