6,7-bis(aminomethyl)-2,3-dihydro-5-(3',4'-dichlorophenyl)-1H-pyrrolizine

Base Information

• Chemical Name: 6,7-bis(aminomethyl)-2,3-dihydro-5-(3',4'-dichlorophenyl)-1H-pyrrolizine
• CAS No.: 147299-46-5
• Molecular Formula: C₁₅H₁₇Cl₂N₃
• Molecular Weight: 310.226

Synonyms:6,7-bis(aminomethyl)-2,3-dihydro-5-(3',4'-dichlorophenyl)-1H-pyrrolizine

Chemical Property of 6,7-bis(aminomethyl)-2,3-dihydro-5-(3',4'-dichlorophenyl)-1H-pyrrolizine

Chemical Property:

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Technology Process of 6,7-bis(aminomethyl)-2,3-dihydro-5-(3',4'-dichlorophenyl)-1H-pyrrolizine

There total 1 articles about 6,7-bis(aminomethyl)-2,3-dihydro-5-(3',4'-dichlorophenyl)-1H-pyrrolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dihydro-5-(3',4'-dichlorophenyl)-1H-pyrrolizine-6,7-dinitrile (147299-45-4) → 6,7-bis(aminomethyl)-2,3-dihydro-5-(3',4'-dichlorophenyl)-1H-pyrrolizine (147299-46-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Yield given; Heating;

DOI:10.1021/ja00062a002

Reference yield: 31.0%

acetic anhydride (108-24-7) + 6,7-bis(aminomethyl)-2,3-dihydro-5-(3',4'-dichlorophenyl)-1H-pyrrolizine (147299-46-5) → 6,7-bis(N'-acetamidomethyl)-2,3-dihydro-5-(3',4'-dichlorophenyl)-1H-pyrrolizine

Guidance literature:

With dmap; triethylamine; In dichloromethane; for 2h;

DOI:10.1021/ja00062a002

Reference yield:

2-fluoro-O6-(2-(p-nitrophenyl)ethyl)-2'-deoxyinosine (132183-39-2) + 6,7-bis(aminomethyl)-2,3-dihydro-5-(3',4'-dichlorophenyl)-1H-pyrrolizine (147299-46-5) → C51H51Cl2N13O12 (147299-49-8)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 25 ℃; for 70h; Yield given;

DOI:10.1021/ja00062a002

upstream raw materials:

2,3-dihydro-5-(3',4'-dichlorophenyl)-1H-pyrrolizine-6,7-dinitrile

Downstream raw materials:

C₅₁H₅₁Cl₂N₁₃O₁₂

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