2-[6-[3,4-Dihydro-4-oxo-8-propyl-2H-1-benzopyran-7-yl)-5-hexynyloxy]benzenepropanoic Acid

Base Information

Chemical Name:2-[6-[3,4-Dihydro-4-oxo-8-propyl-2H-1-benzopyran-7-yl)-5-hexynyloxy]benzenepropanoic Acid
CAS No.:150597-41-4
Molecular Formula:C₂₇H₃₀O₅
Molecular Weight:434.532
Hs Code.:

Synonyms:2-[6-[3,4-Dihydro-4-oxo-8-propyl-2H-1-benzopyran-7-yl)-5-hexynyloxy]benzenepropanoic Acid

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Chemical Property of 2-[6-[3,4-Dihydro-4-oxo-8-propyl-2H-1-benzopyran-7-yl)-5-hexynyloxy]benzenepropanoic Acid

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Technology Process of 2-[6-[3,4-Dihydro-4-oxo-8-propyl-2H-1-benzopyran-7-yl)-5-hexynyloxy]benzenepropanoic Acid

There total 7 articles about 2-[6-[3,4-Dihydro-4-oxo-8-propyl-2H-1-benzopyran-7-yl)-5-hexynyloxy]benzenepropanoic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 150598-27-9
2-[6-(3,4-dihydro-4-oxo-8-propyl-2H-1-benzopyran-7-yl)-5-hexynyloxy]benzenepropanoic acid methyl ester

: 150597-41-4
2-[6-[3,4-Dihydro-4-oxo-8-propyl-2H-1-benzopyran-7-yl)-5-hexynyloxy]benzenepropanoic Acid

Guidance literature:: With acetic acid;

Reference yield:

: 76833-51-7
1-[2-hydroxy-4-(phenylmethoxy)-3-propylphenyl]ethanone

: 150597-41-4
2-[6-[3,4-Dihydro-4-oxo-8-propyl-2H-1-benzopyran-7-yl)-5-hexynyloxy]benzenepropanoic Acid

Guidance literature:: Multi-step reaction with 5 steps

1: p-toluenesulfonic acid monohydrate / methanol; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; water

2: palladium

3: pyridine; trifluoromethanesulfonic acid anhydride / dichloromethane

4: triethylamine / dichlorobis(triphenylphosphine)palladium[II] / N-methyl-acetamide

5: acetic acid

With pyridine; p-toluenesulfonic acid monohydrate; acetic acid; trifluoromethanesulfonic acid anhydride; triethylamine; dichlorobis(triphenylphosphine)palladium[II]; palladium; In N-methyl-acetamide; methanol; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; dichloromethane; water;

Reference yield:

: 928-90-5
5-hexyl-1-ol

: 150597-41-4
2-[6-[3,4-Dihydro-4-oxo-8-propyl-2H-1-benzopyran-7-yl)-5-hexynyloxy]benzenepropanoic Acid

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine / tetrahydrofuran

2: triethylamine / dichlorobis(triphenylphosphine)palladium[II] / N-methyl-acetamide

3: acetic acid

With acetic acid; triethylamine; triphenylphosphine; dichlorobis(triphenylphosphine)palladium[II]; In tetrahydrofuran; N-methyl-acetamide;