2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-isobutyl ester

Base Information

Chemical Name:2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-isobutyl ester
CAS No.:147597-19-1
Molecular Formula:C₂₂H₂₅N₃O₆
Molecular Weight:427.457
Hs Code.:

Synonyms:2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-isobutyl ester

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Chemical Property of 2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-isobutyl ester

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Technology Process of 2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-isobutyl ester

There total 4 articles about 2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-isobutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.3%

: 193539-61-6
(Z)-3-Amino-but-2-enoic acid 2-cyano-ethyl ester

: 89080-63-7
2-(3-nitrobenzylidene)-acetoacetic acid isobutylester

: 147597-19-1
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-isobutyl ester

Guidance literature:: In isopropyl alcohol; for 3h; Heating;
DOI:10.1248/cpb.41.108

Reference yield:

: 7779-75-1
isobutyl acetoacetate

: 147597-19-1
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-isobutyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH, piperidine / benzene / 2 h / Heating

2: 72.3 percent / propan-2-ol / 3 h / Heating

With piperidine; acetic acid; In isopropyl alcohol; benzene;
DOI:10.1248/cpb.41.108

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 147597-19-1
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-cyano-ethyl) ester 5-isobutyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH, piperidine / benzene / 2 h / Heating

2: 72.3 percent / propan-2-ol / 3 h / Heating

With piperidine; acetic acid; In isopropyl alcohol; benzene;
DOI:10.1248/cpb.41.108