(R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoic acid (R)-(+)-α-methylbenzylamine salt

Base Information

Chemical Name:(R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoic acid (R)-(+)-α-methylbenzylamine salt
CAS No.:1313429-33-2
Molecular Formula:C₈H₁₁N*C₁₃H₁₈O₃
Molecular Weight:343.466
Hs Code.:

Synonyms:(R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoic acid (R)-(+)-α-methylbenzylamine salt

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Chemical Property of (R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoic acid (R)-(+)-α-methylbenzylamine salt

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Technology Process of (R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoic acid (R)-(+)-α-methylbenzylamine salt

There total 28 articles about (R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoic acid (R)-(+)-α-methylbenzylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 1616-70-2
2-methyl-3-(3-methoxyphenyl)valeric acid

: 1313429-33-2
(R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoic acid (R)-(+)-α-methylbenzylamine salt

Guidance literature:: In di-isopropyl ether; at 20 - 75 ℃; for 6h;

Reference yield:

: 3886-69-9
(R)-1-phenyl-ethyl-amine

: 1616-70-2
2-methyl-3-(3-methoxyphenyl)valeric acid

: C₈H₁₁N*C₁₃H₁₈O₃

: 1313429-33-2
(R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoic acid (R)-(+)-α-methylbenzylamine salt

: (S),(S)-3-(3-methoxy-phenyl)-2-methyl-pentanoic acid (R)-(+)-α-methylbenzylamine salt

: C₈H₁₁N*C₁₃H₁₈O₃

Guidance literature:: In di-isopropyl ether; at 20 - 75 ℃; for 6h;

Reference yield:

: 591-31-1
3-methoxy-benzaldehyde

: C₈H₁₁N*C₁₃H₁₈O₃

: 1313429-33-2
(R),(R)-3-(3-methoxy-phenyl)-2-methyl-pentanoic acid (R)-(+)-α-methylbenzylamine salt

: (S),(S)-3-(3-methoxy-phenyl)-2-methyl-pentanoic acid (R)-(+)-α-methylbenzylamine salt

: C₈H₁₁N*C₁₃H₁₈O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 6 h / 50 - 60 °C

2.1: tetrahydrofuran / -15 - 25 °C / Inert atmosphere

2.2: 0 - 5 °C

3.1: sodium hydride / toluene / 1 h / 20 °C / Inert atmosphere

3.2: 4 h / 45 - 50 °C

3.3: 0 - 5 °C / pH 1

4.1: lithium chloride / dimethyl sulfoxide / 15 h / 150 - 160 °C

5.1: sodium hydroxide / ethylene glycol / 4 h / 170 - 180 °C

5.2: pH 1

6.1: di-isopropyl ether / 6 h / 20 - 75 °C

With sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; sodium hydroxide; In tetrahydrofuran; di-isopropyl ether; ethylene glycol; dimethyl sulfoxide; toluene;