methyl (N-benzyloxycarbonyl-2-aminoethyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-α-L-idopyranoside)uronate

Base Information

Chemical Name:methyl (N-benzyloxycarbonyl-2-aminoethyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-α-L-idopyranoside)uronate
CAS No.:1364662-67-8
Molecular Formula:C₄₉H₆₀N₄O₁₇
Molecular Weight:977.032
Hs Code.:

methyl (N-benzyloxycarbonyl-2-aminoethyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-α-L-idopyranoside)uronate

Synonyms:methyl (N-benzyloxycarbonyl-2-aminoethyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-α-L-idopyranoside)uronate

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Chemical Property of methyl (N-benzyloxycarbonyl-2-aminoethyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-α-L-idopyranoside)uronate

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Technology Process of methyl (N-benzyloxycarbonyl-2-aminoethyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-α-L-idopyranoside)uronate

There total 6 articles about methyl (N-benzyloxycarbonyl-2-aminoethyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-α-L-idopyranoside)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 77987-49-6
benzyl 2-hydroxyethylcarbamate

: 1364662-63-4
O-(methyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-L-idopyranosuronate)trichloroacetimidate

: 1364662-67-8
methyl (N-benzyloxycarbonyl-2-aminoethyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-α-L-idopyranoside)uronate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;
DOI:10.1039/c2ob06607f

Reference yield:

: C₄₂H₅₉N₃O₁₄Si

: 1364662-67-8
methyl (N-benzyloxycarbonyl-2-aminoethyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-α-L-idopyranoside)uronate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine; dmap / 36 h / 20 °C

2: pyridine hydrofluoride / tetrahydrofuran / 28 h / -15 - 20 °C / Inert atmosphere

3: potassium carbonate / dichloromethane / 6 h / 20 °C

4: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

With pyridine; dmap; pyridine hydrofluoride; trimethylsilyl trifluoromethanesulfonate; potassium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2ob06607f

Reference yield:

: 1380592-26-6
C₄₇H₆₇N₃O₁₅Si

: 1364662-67-8
methyl (N-benzyloxycarbonyl-2-aminoethyl 4-O-(6-O-acetyl-2-azido-3-O-benzyl-2-deoxy-4-O-levulinoyl-α-D-glucopyranosyl)-3-O-benzyl-2-O-pivaloyl-α-L-idopyranoside)uronate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine hydrofluoride / tetrahydrofuran / 28 h / -15 - 20 °C / Inert atmosphere

2: potassium carbonate / dichloromethane / 6 h / 20 °C

3: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

With pyridine hydrofluoride; trimethylsilyl trifluoromethanesulfonate; potassium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2ob06607f