1,3-di-O-acetyl-2-amino-4,6-O-benzylidene-2-deoxy-β-D-glucopyranose hydrochloride

Base Information

Chemical Name:1,3-di-O-acetyl-2-amino-4,6-O-benzylidene-2-deoxy-β-D-glucopyranose hydrochloride
CAS No.:85065-28-7
Molecular Formula:C₁₇H₂₁NO₇*ClH
Molecular Weight:387.817
Hs Code.:

Synonyms:1,3-di-O-acetyl-2-amino-4,6-O-benzylidene-2-deoxy-β-D-glucopyranose hydrochloride

Suppliers and Price of 1,3-di-O-acetyl-2-amino-4,6-O-benzylidene-2-deoxy-β-D-glucopyranose hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-di-O-acetyl-2-amino-4,6-O-benzylidene-2-deoxy-β-D-glucopyranose hydrochloride

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1,3-di-O-acetyl-2-amino-4,6-O-benzylidene-2-deoxy-β-D-glucopyranose hydrochloride

There total 6 articles about 1,3-di-O-acetyl-2-amino-4,6-O-benzylidene-2-deoxy-β-D-glucopyranose hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 85065-27-6
1,3-di-O-acetyl-4,6-O-benzylidene-2-benzylideneamino-2-deoxy-β-D-glucopyranose

: 85065-28-7
1,3-di-O-acetyl-2-amino-4,6-O-benzylidene-2-deoxy-β-D-glucopyranose hydrochloride

Guidance literature:: With hydrogenchloride; In acetone; for 0.25h; ice-bath;
DOI:10.1039/P19840000275

Reference yield:

: 85065-26-5
4,6-O-benzylidene-2-benzylideneamino-2-deoxy-β-D-glucopyranose

: 85065-28-7
1,3-di-O-acetyl-2-amino-4,6-O-benzylidene-2-deoxy-β-D-glucopyranose hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / pyridine

2: 80 percent / 5M HCl / acetone / 0.25 h / ice-bath

With pyridine; hydrogenchloride; In acetone;
DOI:10.1039/P19840000275

Reference yield:

: 90176-39-9
N-(2-deoxy-D-glucopyranos-2-yl)salicylaldimine

: 85065-28-7
1,3-di-O-acetyl-2-amino-4,6-O-benzylidene-2-deoxy-β-D-glucopyranose hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: ZnCl₂

2: pyridine / 16 h / 0 - 20 °C

3: 5M HCl / acetone / 4 °C

With pyridine; hydrogenchloride; zinc(II) chloride; In acetone;
DOI:10.1016/0008-6215(83)88320-7