L-2-(hydroxydipropylmethyl)-1-{[4-(hydroxydipropylmethyl)]phenyl}pyrrolidine

Base Information

Chemical Name:L-2-(hydroxydipropylmethyl)-1-{[4-(hydroxydipropylmethyl)]phenyl}pyrrolidine
CAS No.:1369491-96-2
Molecular Formula:C₂₅H₄₃NO₂
Molecular Weight:389.622
Hs Code.:

Synonyms:L-2-(hydroxydipropylmethyl)-1-{[4-(hydroxydipropylmethyl)]phenyl}pyrrolidine

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Chemical Property of L-2-(hydroxydipropylmethyl)-1-{[4-(hydroxydipropylmethyl)]phenyl}pyrrolidine

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Technology Process of L-2-(hydroxydipropylmethyl)-1-{[4-(hydroxydipropylmethyl)]phenyl}pyrrolidine

There total 3 articles about L-2-(hydroxydipropylmethyl)-1-{[4-(hydroxydipropylmethyl)]phenyl}pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1369491-95-1
C₂₅H₃₅NO₂

: 1369491-96-2
L-2-(hydroxydipropylmethyl)-1-{[4-(hydroxydipropylmethyl)]phenyl}pyrrolidine

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1002/ejic.201101145

Reference yield:

: 195391-98-1,315248-77-2
L-2-(diallylhydroxymethyl)pyrrolidine

: 1369491-96-2
L-2-(hydroxydipropylmethyl)-1-{[4-(hydroxydipropylmethyl)]phenyl}pyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / acetonitrile / 24 h / 30 °C

2: magnesium / diethyl ether / 12 h / 0 - 30 °C

3: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 20 °C

With palladium 10% on activated carbon; hydrogen; magnesium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1002/ejic.201101145

Reference yield:

: 2417-72-3
Methyl 4-(bromomethyl)benzoate

: 1369491-96-2
L-2-(hydroxydipropylmethyl)-1-{[4-(hydroxydipropylmethyl)]phenyl}pyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / acetonitrile / 24 h / 30 °C

2: magnesium / diethyl ether / 12 h / 0 - 30 °C

3: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 3 h / 20 °C

With palladium 10% on activated carbon; hydrogen; magnesium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1002/ejic.201101145