C₅₀H₅₀O₉

Base Information

Chemical Name:C₅₀H₅₀O₉
CAS No.:1585169-39-6
Molecular Formula:C₅₀H₅₀O₉
Molecular Weight:794.942
Hs Code.:

C<sub>50</sub>H<sub>50</sub>O<sub>9</sub>

Synonyms:C₅₀H₅₀O₉

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Chemical Property of C₅₀H₅₀O₉

Chemical Property:

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Technology Process of C₅₀H₅₀O₉

There total 6 articles about C₅₀H₅₀O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1585169-38-5
C₄₃H₄₄O₉

: 100-44-7
benzyl chloride

: 1585169-39-6
C₅₀H₅₀O₉

Guidance literature:: C₄₃H₄₄O₉; benzyl chloride; With sodium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide; at -78 - 20 ℃; Inert atmosphere;

With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ol500725e

Reference yield:

: 1585169-36-3
C₄₃H₄₅BrO₈

: 1585169-39-6
C₅₀H₅₀O₉

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; isopropylmagnesium chloride / tetrahydrofuran; cyclohexane / 0.75 h / -78 - -20 °C

1.2: 0.5 h / -20 °C

2.1: sodium iodide; aluminum (III) chloride / acetonitrile / 1 h / 80 °C / Inert atmosphere

3.1: sodium hexamethyldisilazane / N,N-dimethyl-formamide; tetrahydrofuran / -78 - 20 °C / Inert atmosphere

3.2: 18 h / 20 °C / Inert atmosphere

With aluminum (III) chloride; n-butyllithium; isopropylmagnesium chloride; sodium hexamethyldisilazane; sodium iodide; In tetrahydrofuran; cyclohexane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol500725e

Reference yield:

: 141196-74-9
1-trifluoroacetoxy-2,3,4,6-tetra-O-benzyl-α,β-D-glucopyranoside

: 1585169-39-6
C₅₀H₅₀O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 0 °C

2.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine

3.1: sodium iodide; aluminum (III) chloride / acetonitrile / 1 h / 80 °C / Inert atmosphere

4.1: sodium hexamethyldisilazane / N,N-dimethyl-formamide; tetrahydrofuran / -78 - 20 °C / Inert atmosphere

4.2: 18 h / 20 °C / Inert atmosphere

With aluminum (III) chloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; boron trifluoride diethyl etherate; sodium hexamethyldisilazane; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 1.1: |Friedel-Crafts Alkylation;
DOI:10.1021/ol500725e