(2R,3S)-N-(3-azido-2-hydroxynon-8-enyl)-N-isobutyl-4-methoxybenzenesulfonamide

Base Information

Chemical Name:(2R,3S)-N-(3-azido-2-hydroxynon-8-enyl)-N-isobutyl-4-methoxybenzenesulfonamide
CAS No.:852820-77-0
Molecular Formula:C₂₀H₃₂N₄O₄S
Molecular Weight:424.564
Hs Code.:

Synonyms:(2R,3S)-N-(3-azido-2-hydroxynon-8-enyl)-N-isobutyl-4-methoxybenzenesulfonamide

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Chemical Property of (2R,3S)-N-(3-azido-2-hydroxynon-8-enyl)-N-isobutyl-4-methoxybenzenesulfonamide

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Technology Process of (2R,3S)-N-(3-azido-2-hydroxynon-8-enyl)-N-isobutyl-4-methoxybenzenesulfonamide

There total 8 articles about (2R,3S)-N-(3-azido-2-hydroxynon-8-enyl)-N-isobutyl-4-methoxybenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 852820-78-1
(2R,3S)-3-Azido-1-isobutylamino-non-8-en-2-ol

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 852820-77-0
(2R,3S)-N-(3-azido-2-hydroxynon-8-enyl)-N-isobutyl-4-methoxybenzenesulfonamide

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 23 ℃; for 12.5h;
DOI:10.1021/jm050019i

Reference yield:

: 852820-76-9
(1S,2'R)-2'-(1-azidohept-6-enyl)oxirane

: 852820-77-0
(2R,3S)-N-(3-azido-2-hydroxynon-8-enyl)-N-isobutyl-4-methoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / propan-2-ol / 1.33 h / 90 °C

2: 90 percent / aq. NaHCO₃ / CH₂Cl₂ / 12.5 h / 23 °C

With sodium hydrogencarbonate; In dichloromethane; isopropyl alcohol;
DOI:10.1021/jm050019i

Reference yield:

: 852820-75-8
(2S,3S)-3-azido-non-8-ene-1,2-diol

: 852820-77-0
(2R,3S)-N-(3-azido-2-hydroxynon-8-enyl)-N-isobutyl-4-methoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1-chlorocarbonyl-methylethyl acetate / CHCl₃ / 0.25 h / 23 °C

1.2: 54 percent / NaOMe / tetrahydrofuran / 3 h / 23 °C

2.1: 62 percent / propan-2-ol / 1.33 h / 90 °C

3.1: 90 percent / aq. NaHCO₃ / CH₂Cl₂ / 12.5 h / 23 °C

With 3-acetoxybutyryl chloride; sodium hydrogencarbonate; In dichloromethane; chloroform; isopropyl alcohol;
DOI:10.1021/jm050019i