C₂₃H₃₉NO₂Sn

Base Information

• Chemical Name: C₂₃H₃₉NO₂Sn
• CAS No.: 1204430-99-8
• Molecular Formula: C₂₃H₃₉NO₂Sn
• Molecular Weight: 480.278
• Mol file: 1204430-99-8.mol

Synonyms:C₂₃H₃₉NO₂Sn

Chemical Property of C₂₃H₃₉NO₂Sn

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₃₉NO₂Sn

There total 1 articles about C₂₃H₃₉NO₂Sn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

N-(4-methoxyphenyl)-2-methylacrylamide (7274-71-7) + tributyltin chloride (1461-22-9) → C23H39NO2Sn (1204430-99-8)

Guidance literature:

N-(4-methoxyphenyl)-2-methylacrylamide; With potassium tert-butylate; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h; Inert atmosphere;

tributyltin chloride; In tetrahydrofuran; hexane; for 1h; Inert atmosphere;

DOI:10.1039/c4ob01508h

Reference yield: 99.0%

methyl 2-oxo-2-phenylacetate (15206-55-0) + C23H39NO2Sn (1204430-99-8) → C20H21NO5

Guidance literature:

methyl 2-oxo-2-phenylacetate; With indium(III) triflate; (S,S)-2,6-bis(4-phenyl-2-oxazolinyl)pyridine; In acetonitrile; at 20 ℃; Molecular sieve; Inert atmosphere;

C₂₃H₃₉NO₂Sn; In acetonitrile; at 20 ℃; for 15h; enantioselective reaction; Molecular sieve; Inert atmosphere;

DOI:10.1039/c4ob01508h

Reference yield: 97.0%

C23H39NO2Sn (1204430-99-8) + benzyl oxo(phenyl)acetate (62977-82-6) → C26H25NO5

Guidance literature:

benzyl oxo(phenyl)acetate; With indium(III) triflate; (S,S)-2,6-bis(4-phenyl-2-oxazolinyl)pyridine; In acetonitrile; at 20 ℃; Molecular sieve; Inert atmosphere;

C₂₃H₃₉NO₂Sn; In acetonitrile; at 20 ℃; for 13h; enantioselective reaction; Molecular sieve; Inert atmosphere;

DOI:10.1039/c4ob01508h

upstream raw materials:

N-(4-methoxyphenyl)-2-methylacrylamide

tributyltin chloride

Downstream raw materials:

(S)-4-hydroxy-N-(4-methoxyphenyl)-2-methylene-4-phenylbutanamide

Refernces