2-(3-oxetan-3-yl-phenyl)-ethanol

Base Information

Chemical Name:2-(3-oxetan-3-yl-phenyl)-ethanol
CAS No.:1298046-65-7
Molecular Formula:C₁₁H₁₄O₂
Molecular Weight:178.231
Hs Code.:

Synonyms:2-(3-oxetan-3-yl-phenyl)-ethanol

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Chemical Property of 2-(3-oxetan-3-yl-phenyl)-ethanol

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Technology Process of 2-(3-oxetan-3-yl-phenyl)-ethanol

There total 3 articles about 2-(3-oxetan-3-yl-phenyl)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1298046-64-6
tert-butyl-dimethyl-[2-(3-oxetan-3-yl-phenyl)-ethoxy]-silane

: 1298046-65-7
2-(3-oxetan-3-yl-phenyl)-ethanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 249937-07-3
[2‐(3‐bromophenyl)ethoxy](tert‐butyl)dimethylsilane

: 1298046-65-7
2-(3-oxetan-3-yl-phenyl)-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / n-heptane; tetrahydrofuran / 1 h / -70 °C / Inert atmosphere

1.2: 0.5 h / -70 °C / Inert atmosphere

1.3: -20 °C / Inert atmosphere

2.1: (1R,2R)-2-aminocyclohexanol; nickel(II) iodide; sodium hexamethyldisilazane / isopropyl alcohol / 0.17 h / 20 °C / Inert atmosphere; Microwave irradiation

2.2: 0.5 h / 80 °C / Inert atmosphere; Microwave irradiation

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

With nickel(II) iodide; n-butyllithium; (1R,2R)-2-aminocyclohexanol; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; In tetrahydrofuran; n-heptane; isopropyl alcohol;

Reference yield:

: 604768-85-6
3-(2-(tert-butyl)dimethylsilyloxyethyl)phenylboronic acid

: 1298046-65-7
2-(3-oxetan-3-yl-phenyl)-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: (1R,2R)-2-aminocyclohexanol; nickel(II) iodide; sodium hexamethyldisilazane / isopropyl alcohol / 0.17 h / 20 °C / Inert atmosphere; Microwave irradiation

1.2: 0.5 h / 80 °C / Inert atmosphere; Microwave irradiation

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

With nickel(II) iodide; (1R,2R)-2-aminocyclohexanol; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; In tetrahydrofuran; isopropyl alcohol;