(3-Bromophenethoxy)(tert-butyl)dimethylsilane

Base Information

Chemical Name:(3-Bromophenethoxy)(tert-butyl)dimethylsilane
CAS No.:249937-07-3
Molecular Formula:C14H23BrOSi
Molecular Weight:315.326
Hs Code.:2931900090
DSSTox Substance ID:DTXSID10467903
Mol file:249937-07-3.mol

Synonyms:(3-Bromophenethoxy)(tert-butyl)dimethylsilane;249937-07-3;2-(3-bromophenyl)ethoxy-tert-butyl-dimethylsilane;(3-bromophenethyloxy)(tert-butyl)dimethylsilane;[2-(3-bromophenyl)ethoxy](tert-butyl)dimethylsilane;1-Bromo-3-[2-(tert-butyldimethylsilyloxy)ethyl]benzene;SCHEMBL333905;DTXSID10467903;Silane, [2-(3-bromophenyl)ethoxy](1,1-dimethylethyl)dimethyl-;ZJA93707;MFCD09027279;AKOS015834650;BS-22126;CS-0212302;3-(2-tert-butyldimethylsiloxyethyl)bromobenzene;3-(2-tert-butyl-dimethylsiloxyethl) bromobenzene;3-(2-tert-butyl-dimethylsiloxyethyl)bromobenzene;A877744;J-501188;[2-(3-bromophenyl)ethoxy] (tert-butyl)dimethylsilane;[2-(3-bromo-phenyl)-ethoxy]-tert-butyl-dimethyl-silane;3-Bromophenethyl alcohol, tert-butyldimethylsilyl ether;1-Bromo-3-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]benzene;Benzene, 1-bromo-3-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]-

Suppliers and Price of (3-Bromophenethoxy)(tert-butyl)dimethylsilane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(3-Bromophenethoxy)(tert-butyl)dimethylsilane
1g
$ 200.00

SynQuest Laboratories
1-Bromo-3-[2-(tert-butyldimethylsilyloxy)ethyl]benzene 98%
5 g
$ 592.00

SynQuest Laboratories
1-Bromo-3-[2-(tert-butyldimethylsilyloxy)ethyl]benzene 98%
1 g
$ 136.00

Matrix Scientific
(3-Bromophenethoxy)(tert-butyl)dimethylsilane 95+%
250mg
$ 152.00

Matrix Scientific
(3-Bromophenethoxy)(tert-butyl)dimethylsilane 95+%
1g
$ 336.00

Crysdot
(3-Bromophenethoxy)(tert-butyl)dimethylsilane 97%
5g
$ 339.00

Chemenu
(3-Bromophenethoxy)(tert-butyl)dimethylsilane 97%
5g
$ 320.00

American Custom Chemicals Corporation
1-BROMO-3-[2-(TERT-BUTYLDIMETHYLSILYLOXY)ETHYL]BENZENE 95.00%
5G
$ 1223.72

American Custom Chemicals Corporation
1-BROMO-3-[2-(TERT-BUTYLDIMETHYLSILYLOXY)ETHYL]BENZENE 95.00%
1G
$ 701.20

AK Scientific
(3-Bromophenethyloxy)(tert-butyl)dimethylsilane
5g
$ 531.00

Total 12 raw suppliers

Chemical Property of (3-Bromophenethoxy)(tert-butyl)dimethylsilane

Chemical Property:

Vapor Pressure:0.001mmHg at 25°C
Refractive Index:1.496
Boiling Point:317.782 °C at 760 mmHg
Flash Point:145.99 °C
PSA：9.23000
Density:1.128 g/cm³
LogP:5.01340
Storage Temp.:2-8°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:314.07015
Heavy Atom Count:17
Complexity:235

Purity/Quality:

97% ^*data from raw suppliers

(3-Bromophenethoxy)(tert-butyl)dimethylsilane ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)[Si](C)(C)OCCC1=CC(=CC=C1)Br

Technology Process of (3-Bromophenethoxy)(tert-butyl)dimethylsilane

There total 2 articles about (3-Bromophenethoxy)(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 28229-69-8
2-(3-bromophenyl)ethan-1-ol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 249937-07-3
[2‐(3‐bromophenyl)ethoxy](tert‐butyl)dimethylsilane

Guidance literature:: With 1H-imidazole; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 1878-67-7
3-Bromophenylacetic acid

: 249937-07-3
[2‐(3‐bromophenyl)ethoxy](tert‐butyl)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 9.0 g / diborane / tetrahydrofuran / 16 h / 20 °C

2: 6.0 g / 4-(dimethylamino)pyridine; Et₃N / CH₂Cl₂ / 1 h

With dmap; triethylamine; diborane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm050736c