(2S,3R)-3-Acetoxy-2-hydroxy-3-(4-methoxy-phenyl)-propionic acid ethyl ester

Base Information

Chemical Name:(2S,3R)-3-Acetoxy-2-hydroxy-3-(4-methoxy-phenyl)-propionic acid ethyl ester
CAS No.:182187-05-9
Molecular Formula:C₁₄H₁₈O₆
Molecular Weight:282.293
Hs Code.:

Synonyms:(2S,3R)-3-Acetoxy-2-hydroxy-3-(4-methoxy-phenyl)-propionic acid ethyl ester

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Chemical Property of (2S,3R)-3-Acetoxy-2-hydroxy-3-(4-methoxy-phenyl)-propionic acid ethyl ester

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Technology Process of (2S,3R)-3-Acetoxy-2-hydroxy-3-(4-methoxy-phenyl)-propionic acid ethyl ester

There total 4 articles about (2S,3R)-3-Acetoxy-2-hydroxy-3-(4-methoxy-phenyl)-propionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: C₁₆H₁₇⁽²⁾H₃O₇

: 182187-05-9
(2S,3R)-3-Acetoxy-2-hydroxy-3-(4-methoxy-phenyl)-propionic acid ethyl ester

Guidance literature:: With AmanoPS; sodium phosphate buffer; In Petroleum ether; benzene; at 25 ℃; for 2h; pH=7.0;
DOI:10.1021/jo990598x

Reference yield: 51.0%

: 2,3-Diacetoxy-3-(4-methoxy-phenyl)-propionic acid ethyl ester

: 182187-05-9
(2S,3R)-3-Acetoxy-2-hydroxy-3-(4-methoxy-phenyl)-propionic acid ethyl ester

: 182509-56-4
(2R,3S)-2,3-Diacetoxy-3-(4-methoxy-phenyl)-propionic acid ethyl ester

Guidance literature:: With sodium phosphate; In 2,2,4-trimethylpentane; benzene; at 25 ℃; for 180h; Amano PS lipase, pH 7.0;
DOI:10.1021/jo960835l

Reference yield:

: 24393-56-4
ethyl (E)-3-(4-methoxyphenyl)prop-2-enoate

: 182187-05-9
(2S,3R)-3-Acetoxy-2-hydroxy-3-(4-methoxy-phenyl)-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / OsO₄, aq. NMO / 2-methyl-propan-2-ol / 48 h / Ambient temperature

2: 5.2 percent Spectr_. / petroleum ether; benzene / 96 h / 25 °C / Amano-PS lipase

3: 42 percent / aq. sodium phosphate / 2,2,4-trimethyl-pentane; benzene / 180 h / 25 °C / Amano PS lipase, pH 7.0

With osmium(VIII) oxide; N-methyl-2-indolinone; sodium phosphate; In 2,2,4-trimethylpentane; Petroleum ether; tert-butyl alcohol; benzene;
DOI:10.1021/jo960835l