dimethyl 2-(N-((2,3-dimethyl-1H-indol-5-yl)(phenyl)methyl)-4-methylphenylsulfonamido)malonate

Base Information

• Chemical Name: dimethyl 2-(N-((2,3-dimethyl-1H-indol-5-yl)(phenyl)methyl)-4-methylphenylsulfonamido)malonate
• CAS No.: 1538607-34-9
• Molecular Formula: C₂₉H₃₀N₂O₆S
• Molecular Weight: 534.633

Synonyms:dimethyl 2-(N-((2,3-dimethyl-1H-indol-5-yl)(phenyl)methyl)-4-methylphenylsulfonamido)malonate

Chemical Property of dimethyl 2-(N-((2,3-dimethyl-1H-indol-5-yl)(phenyl)methyl)-4-methylphenylsulfonamido)malonate

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Technology Process of dimethyl 2-(N-((2,3-dimethyl-1H-indol-5-yl)(phenyl)methyl)-4-methylphenylsulfonamido)malonate

There total 5 articles about dimethyl 2-(N-((2,3-dimethyl-1H-indol-5-yl)(phenyl)methyl)-4-methylphenylsulfonamido)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2,3-dimethylindole (91-55-4) + (1S,3aR,8bR)-dimethyl 3a,8b-dimethyl-1-phenyl-2-tosyl-1,3a,4,8b-tetrahydropyrrolo[3,4-b]indole-3,3(2H)-dicarboxylate → dimethyl 2-(N-((2,3-dimethyl-1H-indol-6-yl)(phenyl)methyl)-4-methylphenylsulfonamido)malonate (1538607-33-8) + dimethyl 2-(N-((2,3-dimethyl-1H-indol-5-yl)(phenyl)methyl)-4-methylphenylsulfonamido)malonate (1538607-34-9)

Guidance literature:

With scandium tris(trifluoromethanesulfonate); In toluene; at 20 ℃; for 1h; Solvent; Time; Inert atmosphere; Molecular sieve;

DOI:10.1021/jo402511b

Reference yield: 80.0%

2,3-dimethylindole (91-55-4) + dimethyl 3-phenyl-1-tosylaziridine-2,2-dicarboxylate (1132667-77-6) → dimethyl 2-(N-((2,3-dimethyl-1H-indol-6-yl)(phenyl)methyl)-4-methylphenylsulfonamido)malonate (1538607-33-8) + dimethyl 2-(N-((2,3-dimethyl-1H-indol-5-yl)(phenyl)methyl)-4-methylphenylsulfonamido)malonate (1538607-34-9)

Guidance literature:

With scandium tris(trifluoromethanesulfonate); In toluene; at 20 ℃; for 0.5h; Inert atmosphere; Molecular sieve;

DOI:10.1021/jo402511b

Reference yield: 73.17%

2,3-dimethylindole (91-55-4) + dimethyl 3-phenyl-1-tosylaziridine-2,2-dicarboxylate (1132667-77-6) → (1S,3aR,8bR)-dimethyl 3a,8b-dimethyl-1-phenyl-2-tosyl-1,3a,4,8b-tetrahydropyrrolo[3,4-b]indole-3,3(2H)-dicarboxylate + dimethyl 2-(N-((2,3-dimethyl-1H-indol-6-yl)(phenyl)methyl)-4-methylphenylsulfonamido)malonate (1538607-33-8) + dimethyl 2-(N-((2,3-dimethyl-1H-indol-5-yl)(phenyl)methyl)-4-methylphenylsulfonamido)malonate (1538607-34-9)

Guidance literature:

With nickel(II) perchlorate hexahydrate; In toluene; at 20 ℃; for 3h; Reagent/catalyst; Inert atmosphere; Molecular sieve;

DOI:10.1021/jo402511b

upstream raw materials:

2,3-dimethylindole

dimethyl 3-phenyl-1-tosylaziridine-2,2-dicarboxylate

1,2,3,4-tetrahydrocarbazole

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