p-methoxyphenyl 2-azido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-α-D-mannopyranoside

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Chemical Name:p-methoxyphenyl 2-azido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-α-D-mannopyranoside
CAS No.:402831-55-4
Molecular Formula:C₁₉H₂₃N₃O₈S
Molecular Weight:453.473
Hs Code.:

Synonyms:p-methoxyphenyl 2-azido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-methoxyphenyl 2-azido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-α-D-mannopyranoside

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Technology Process of p-methoxyphenyl 2-azido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-α-D-mannopyranoside

There total 3 articles about p-methoxyphenyl 2-azido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 696-63-9
4-Methoxybenzenethiol

: 139066-49-2
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-α/β-D-mannopyranose

: 402831-55-4
p-methoxyphenyl 2-azido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-α-D-mannopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 35 ℃;
DOI:10.1016/S0040-4039(01)01880-9

Reference yield:

: 97604-58-5
2-azido-2-deoxy-D-mannopyranose

: 402831-55-4
p-methoxyphenyl 2-azido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / DMAP

2: 59 percent / BF₃*OEt₂ / CH₂Cl₂ / 35 °C

With pyridine; boron trifluoride diethyl etherate; dmap; In dichloromethane;
DOI:10.1016/S0040-4039(01)01880-9

Reference yield:

: 4710-95-6,6730-09-2,14131-59-0,14131-62-5,14131-63-6,14131-65-8,14131-67-0,14257-79-5,19124-46-0,20706-90-5,91673-92-6
D-mannosamine hydrochloride

: 402831-55-4
p-methoxyphenyl 2-azido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: TfN₃; K₂CO₃ / CuSO₄ / H₂O; methanol; CH₂Cl₂

2: pyridine / DMAP

3: 59 percent / BF₃*OEt₂ / CH₂Cl₂ / 35 °C

With pyridine; triflic azide; boron trifluoride diethyl etherate; potassium carbonate; dmap; copper(II) sulfate; In methanol; dichloromethane; water;
DOI:10.1016/S0040-4039(01)01880-9