4-MeC₆H₃Me=NNCSNHEt

Base Information

Chemical Name:4-MeC₆H₃Me=NNCSNHEt
CAS No.:433925-83-8
Molecular Formula:C₁₂H₁₇N₃S
Molecular Weight:235.353
Hs Code.:

4-MeC<sub>6</sub>H<sub>3</sub>Me=NNCSNHEt

Synonyms:4-MeC₆H₃Me=NNCSNHEt

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Chemical Property of 4-MeC₆H₃Me=NNCSNHEt

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Technology Process of 4-MeC₆H₃Me=NNCSNHEt

There total 1 articles about 4-MeC₆H₃Me=NNCSNHEt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 13431-34-0
N-ethylthiosemicarbazide

: 122-00-9
para-methylacetophenone

: 433925-83-8
4-MeC₆H₃Me=NNCSNHEt

Guidance literature:: With hydrogenchloride; at 20 ℃;
DOI:10.1002/1099-0682(200203)2002:3<613::AID-EJIC613>3.0.CO;2-A

Reference yield: 87.0%

: 10025-98-6
potassium tetrachloropalladate(II)

: 433925-83-8
4-MeC₆H₃Me=NNCSNHEt

: [Pd(4-MeC₆H₃CMe=NNCSNHEt)]4

Guidance literature:: In ethanol; water; ethanol added to soln. of Pd complex salt in water under stirring, addn.of the thiosemicarbazone, stirred at room temp. for 48 h; ppt. filtered off, washed with ethanol and dried; elem. anal.;
DOI:10.1002/1099-0682(200203)2002:3<613::AID-EJIC613>3.0.CO;2-A

Reference yield: 63.0%

: 3375-31-3
palladium diacetate

: 433925-83-8
4-MeC₆H₃Me=NNCSNHEt

: [Pd(4-MeC₆H₃CMe=NNCSNHEt)]4

Guidance literature:: In acetic acid; Pd acetate and the thiosemicarbazone added to glacial acetic acid, heated at 60°C for 8 h; cooled to room temp., evapd. under vac., residue extracted with CH2Cl2, combined extracts dried over Na2SO4, filtered, concd. in vac., chromy. (silical gel, CH2Cl2/EtOH(1%)); elem. anal.;
DOI:10.1002/1099-0682(200203)2002:3<613::AID-EJIC613>3.0.CO;2-A