C₄₄H₅₀FN₃O₁₆

Base Information

Chemical Name:C₄₄H₅₀FN₃O₁₆
CAS No.:1407186-55-3
Molecular Formula:C₄₄H₅₀FN₃O₁₆
Molecular Weight:895.89
Hs Code.:

C<sub>44</sub>H<sub>50</sub>FN<sub>3</sub>O<sub>16</sub>

Synonyms:C₄₄H₅₀FN₃O₁₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₄H₅₀FN₃O₁₆

Chemical Property:

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Technology Process of C₄₄H₅₀FN₃O₁₆

There total 5 articles about C₄₄H₅₀FN₃O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1407186-54-2
C₄₄H₅₁N₃O₁₇

: 1407186-55-3
C₄₄H₅₀FN₃O₁₆

Guidance literature:: With diethylamino-sulfur trifluoride; In 1,2-dichloro-ethane; at -5 - 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/anie.201204083

Reference yield:

: 7205-49-4
paromomycin sulfate

: 1407186-55-3
C₄₄H₅₀FN₃O₁₆

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride / methanol / Reflux

2: sodium carbonate / water; acetone; toluene / 4 h / 5 - 20 °C

3: dmap; triethylamine / N,N-dimethyl-formamide / 1 h / -5 °C / Inert atmosphere

4: dmap; pyridine / 24 h / 20 °C / Inert atmosphere

5: pyridine hydrogenfluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

6: diethylamino-sulfur trifluoride / 1,2-dichloro-ethane / 5 h / -5 - 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; dmap; diethylamino-sulfur trifluoride; sodium carbonate; pyridine hydrogenfluoride; triethylamine; In tetrahydrofuran; methanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1002/anie.201204083

Reference yield:

: 18685-97-7,68422-90-2,74081-52-0
paromamine trihydrochloride

: 1407186-55-3
C₄₄H₅₀FN₃O₁₆

Guidance literature:: Multi-step reaction with 5 steps

1: sodium carbonate / water; acetone; toluene / 4 h / 5 - 20 °C

2: dmap; triethylamine / N,N-dimethyl-formamide / 1 h / -5 °C / Inert atmosphere

3: dmap; pyridine / 24 h / 20 °C / Inert atmosphere

4: pyridine hydrogenfluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

5: diethylamino-sulfur trifluoride / 1,2-dichloro-ethane / 5 h / -5 - 20 °C / Inert atmosphere

With pyridine; dmap; diethylamino-sulfur trifluoride; sodium carbonate; pyridine hydrogenfluoride; triethylamine; In tetrahydrofuran; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1002/anie.201204083