O²-acetoxymethyl-1-(N-ethyl-N-methylamino)diazen-1-ium-1,2-diolate (E)-2-(4-fluorophenyl)-3-(4-methanesulfonylphenyl)acrylate

Base Information

• Chemical Name: O²-acetoxymethyl-1-(N-ethyl-N-methylamino)diazen-1-ium-1,2-diolate (E)-2-(4-fluorophenyl)-3-(4-methanesulfonylphenyl)acrylate
• CAS No.: 1029146-29-9
• Molecular Formula: C₂₂H₂₄FN₃O₈S
• Molecular Weight: 509.512
• Mol file: 1029146-29-9.mol

Synonyms:O²-acetoxymethyl-1-(N-ethyl-N-methylamino)diazen-1-ium-1,2-diolate (E)-2-(4-fluorophenyl)-3-(4-methanesulfonylphenyl)acrylate

Chemical Property of O²-acetoxymethyl-1-(N-ethyl-N-methylamino)diazen-1-ium-1,2-diolate (E)-2-(4-fluorophenyl)-3-(4-methanesulfonylphenyl)acrylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of O²-acetoxymethyl-1-(N-ethyl-N-methylamino)diazen-1-ium-1,2-diolate (E)-2-(4-fluorophenyl)-3-(4-methanesulfonylphenyl)acrylate

There total 1 articles about O²-acetoxymethyl-1-(N-ethyl-N-methylamino)diazen-1-ium-1,2-diolate (E)-2-(4-fluorophenyl)-3-(4-methanesulfonylphenyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

O2-acetoxymethyl 1-[N-(2-methylsulfonyloxyethyl)-N-methylamino]diazen-1-ium-1,2-diolate (742081-73-8) + (E)-2-(4-Fluoro-phenyl)-3-(4-methanesulfonyl-phenyl)-acrylic acid (914800-36-5) → O2-acetoxymethyl-1-(N-ethyl-N-methylamino)diazen-1-ium-1,2-diolate (E)-2-(4-fluorophenyl)-3-(4-methanesulfonylphenyl)acrylate (1029146-29-9)

Guidance literature:

(E)-2-(4-Fluoro-phenyl)-3-(4-methanesulfonyl-phenyl)-acrylic acid; With sodium carbonate; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 25 ℃; for 19h;

O²-acetoxymethyl 1-[N-(2-methylsulfonyloxyethyl)-N-methylamino]diazen-1-ium-1,2-diolate; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 25 ℃; for 72h; Further stages.;

DOI:10.1016/j.bmc.2007.12.006

upstream raw materials:

O²-acetoxymethyl 1-[N-(2-methylsulfonyloxyethyl)-N-methylamino]diazen-1-ium-1,2-diolate

(E)-2-(4-Fluoro-phenyl)-3-(4-methanesulfonyl-phenyl)-acrylic acid