(hydridotris(pyrazol-1-yl)borate)nitrosylruthenium(CCC(Ph)2OH)Cl

Base Information

Chemical Name:(hydridotris(pyrazol-1-yl)borate)nitrosylruthenium(CCC(Ph)2OH)Cl
CAS No.:600698-57-5
Molecular Formula:C₂₄H₂₁BClN₇O₂Ru
Molecular Weight:586.81
Hs Code.:

Synonyms:(hydridotris(pyrazol-1-yl)borate)nitrosylruthenium(CCC(Ph)2OH)Cl

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Chemical Property of (hydridotris(pyrazol-1-yl)borate)nitrosylruthenium(CCC(Ph)2OH)Cl

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Technology Process of (hydridotris(pyrazol-1-yl)borate)nitrosylruthenium(CCC(Ph)2OH)Cl

There total 1 articles about (hydridotris(pyrazol-1-yl)borate)nitrosylruthenium(CCC(Ph)2OH)Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 137729-45-4
[(hydridotris(pyrazolyl)borato)RuCl₂(NO)]

: 3923-52-2
1,1-diphenyl-2-propyn-1-ol

: 600698-57-5
(hydridotris(pyrazol-1-yl)borate)nitrosylruthenium(CCC(Ph)2OH)Cl

Guidance literature:: With N(CH₂CH₃)3; In not given; react. of ruthenium complex with excess alkyne;
DOI:10.1021/om0303597

Reference yield: 86.0%

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 600698-57-5
(hydridotris(pyrazol-1-yl)borate)nitrosylruthenium(CCC(Ph)2OH)Cl

: 603-35-0
triphenylphosphine

: [(hydridotris(pyrazol-1-yl)borate)nitrosylruthenium(C(PPh₃)CCPh₂)Cl]BF₄

Guidance literature:: In tetrahydrofuran; under N2; PPh3 and HBF4*Et2O added to THF soln. of Ru complex (molar ratio 1:1:1); stirred at room temp. for 2 h; solvent removed in vac.; recrystd. from CH2Cl2-Et2O; elem. anal.;
DOI:10.1039/b415483e

Reference yield: 65.0%

: 600698-57-5
(hydridotris(pyrazol-1-yl)borate)nitrosylruthenium(CCC(Ph)2OH)Cl

: 38177-85-4
1-(buta-1,3-diyn-1-yl)-4-methylbenzene

: [(HB(pyrazol-1-yl)3)Ru(CCCCC₆H₄Me)(CCC(OH)Ph₂)(NO)]

Guidance literature:: With Et₃N; copper(l) iodide; In dichloromethane; (N2); soln. of alkyne in CH2Cl2, CuI and Et3N were added to soln. of Ru complex in CH2Cl2; refluxed for 3 h; volatiles removed; chromd. (silica gel, CH2Cl2); elem. anal.;
DOI:10.1021/om701028r