4-TRIMETHYLSILYLBENZALDEHYDE

Base Information

• Chemical Name: 4-TRIMETHYLSILYLBENZALDEHYDE
• CAS No.: 2199-32-8
• Molecular Formula: C10H14 O Si
• Molecular Weight: 178.306
• Hs Code.: 2931900090
• Mol file: 2199-32-8.mol

Synonyms:Benzaldehyde,p-(trimethylsilyl)- (6CI,7CI,8CI); 4-(Trimethylsilyl)benzaldehyde;p-(Trimethylsilyl)benzaldehyde

Chemical Property of 4-TRIMETHYLSILYLBENZALDEHYDE

Chemical Property:

• Melting Point: 109-110 °C(Solv: ligroine (8032-32-4))
• Boiling Point: 119 °C(Press: 15 Torr)
• PSA: 17.07000
• Density: 0.9960 g/cm3(Temp: 425 °C)
• LogP: 2.04430
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-(Trimethylsilyl)benzaldehyde 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-TRIMETHYLSILYLBENZALDEHYDE

There total 19 articles about 4-TRIMETHYLSILYLBENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-bromo-4-(trimethylsilyl)benzene (6999-03-7) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 4-trimethylsilylbenzaldehyde (2199-32-8)

Guidance literature:

1-bromo-4-(trimethylsilyl)benzene; With n-butyllithium; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; at -78 - -70 ℃; for 0.25h;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -78 - -68 ℃; for 0.25h;

Reference yield: 100.0%

1-bromo-4-(trimethylsilyl)benzene (6999-03-7) → 4-trimethylsilylbenzaldehyde (2199-32-8)

Guidance literature:

1-bromo-4-(trimethylsilyl)benzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -70 ℃; for 0.25h;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at -78 - -68 ℃; for 0.25h;

Reference yield: 99.0%

→ 4-trimethylsilylbenzaldehyde (2199-32-8)

Guidance literature:

upstream raw materials:

(4-(bromomethyl)phenyl)trimethylsilane

(4-dibromomethyl-phenyl)-trimethyl-silane

formic acid ethyl ester

[4-(trimethylsilyl)phenyl]magnesium bromide

Downstream raw materials:

4-(trimethylsilyl)benzoic acid

4-[(E)-2-(4-Trimethylsilanyl-phenyl)-vinyl]-benzonitrile

[4-(2,2-dibromo-vinyl)-phenyl]-trimethyl-silane