4-(4-methoxyphenyl)-9-(4-(diphenylamino)phenyl)naphtho[2,3-c][1,2,5]thiadiazole

Base Information

Chemical Name:4-(4-methoxyphenyl)-9-(4-(diphenylamino)phenyl)naphtho[2,3-c][1,2,5]thiadiazole
CAS No.:1321600-46-7
Molecular Formula:C₃₅H₂₅N₃OS
Molecular Weight:535.669
Hs Code.:

Synonyms:4-(4-methoxyphenyl)-9-(4-(diphenylamino)phenyl)naphtho[2,3-c][1,2,5]thiadiazole

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Chemical Property of 4-(4-methoxyphenyl)-9-(4-(diphenylamino)phenyl)naphtho[2,3-c][1,2,5]thiadiazole

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Technology Process of 4-(4-methoxyphenyl)-9-(4-(diphenylamino)phenyl)naphtho[2,3-c][1,2,5]thiadiazole

There total 3 articles about 4-(4-methoxyphenyl)-9-(4-(diphenylamino)phenyl)naphtho[2,3-c][1,2,5]thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.2%

: 1321600-45-6
4-(4-(diphenylamino)phenyl)-9-bromonaphtho[2,3-c][1,2,5]thiadiazole

: 5720-07-0
4-methoxyphenylboronic acid

: 1321600-46-7
4-(4-methoxyphenyl)-9-(4-(diphenylamino)phenyl)naphtho[2,3-c][1,2,5]thiadiazole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene; at 100 ℃; for 12h; Inert atmosphere; Darkness;
DOI:10.1039/c1jm11204j

Reference yield:

: 18557-22-7
4,9-dibromonaphtho-[2,3-c][1,2,5]thiadiazole

: 1321600-46-7
4-(4-methoxyphenyl)-9-(4-(diphenylamino)phenyl)naphtho[2,3-c][1,2,5]thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 24 h / 100 °C / Darkness

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; toluene / 12 h / 100 °C / Inert atmosphere; Darkness

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene;
DOI:10.1039/c1jm11204j

Reference yield:

: diphenyl-(4-tributylstannanyl-phenyl)-amine

: 1321600-46-7
4-(4-methoxyphenyl)-9-(4-(diphenylamino)phenyl)naphtho[2,3-c][1,2,5]thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 24 h / 100 °C / Darkness

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; toluene / 12 h / 100 °C / Inert atmosphere; Darkness

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene;
DOI:10.1039/c1jm11204j