diethyl (2E)-2-[{2-[(anilinocarbonyl)hydrazono]-1-[(dimethylamino)carbonyl]propyl}(cyclohexyl)amino]but-2-enedioate

Base Information

Chemical Name:diethyl (2E)-2-[{2-[(anilinocarbonyl)hydrazono]-1-[(dimethylamino)carbonyl]propyl}(cyclohexyl)amino]but-2-enedioate
CAS No.:1188967-14-7
Molecular Formula:C₂₇H₃₉N₅O₆
Molecular Weight:529.637
Hs Code.:

Synonyms:diethyl (2E)-2-[{2-[(anilinocarbonyl)hydrazono]-1-[(dimethylamino)carbonyl]propyl}(cyclohexyl)amino]but-2-enedioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl (2E)-2-[{2-[(anilinocarbonyl)hydrazono]-1-[(dimethylamino)carbonyl]propyl}(cyclohexyl)amino]but-2-enedioate

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Technology Process of diethyl (2E)-2-[{2-[(anilinocarbonyl)hydrazono]-1-[(dimethylamino)carbonyl]propyl}(cyclohexyl)amino]but-2-enedioate

There total 3 articles about diethyl (2E)-2-[{2-[(anilinocarbonyl)hydrazono]-1-[(dimethylamino)carbonyl]propyl}(cyclohexyl)amino]but-2-enedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1188966-95-1
3-[(anilinocarbonyl)hydrazono]-2-(cyclohexylamino)-N,N-dimethylbutanamide

: 762-21-0
acetylenedicarboxylic acid diethyl ester

: 1188967-14-7
diethyl (2E)-2-[{2-[(anilinocarbonyl)hydrazono]-1-[(dimethylamino)carbonyl]propyl}(cyclohexyl)amino]but-2-enedioate

Guidance literature:: In ethanol; Reflux;
DOI:10.1002/adsc.200800807

Reference yield:

: 1027008-08-7
4-dimethylaminocarbonyl-3-methyl-1-phenylaminocarbonyl-1,2-diaza-1,3-butadiene

: 1188967-14-7
diethyl (2E)-2-[{2-[(anilinocarbonyl)hydrazono]-1-[(dimethylamino)carbonyl]propyl}(cyclohexyl)amino]but-2-enedioate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 20 °C

2: ethanol / Reflux

In tetrahydrofuran; ethanol; 1: Michael addition;
DOI:10.1002/adsc.201000796

Reference yield:

: 108-91-8,157973-60-9
cyclohexylamine

: 1188967-14-7
diethyl (2E)-2-[{2-[(anilinocarbonyl)hydrazono]-1-[(dimethylamino)carbonyl]propyl}(cyclohexyl)amino]but-2-enedioate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 20 °C

2: ethanol / Reflux

In tetrahydrofuran; ethanol; 1: Michael addition;
DOI:10.1002/adsc.201000796