4-(5-(4-(dihexylamino)phenyl)thiophene-2-yl)-1-methylpyridinium trifluoromethanesulfonate

Base Information

Chemical Name:4-(5-(4-(dihexylamino)phenyl)thiophene-2-yl)-1-methylpyridinium trifluoromethanesulfonate
CAS No.:1236567-78-4
Molecular Formula:CF₃O₃S*C₂₈H₃₉N₂S
Molecular Weight:584.767
Hs Code.:

Synonyms:4-(5-(4-(dihexylamino)phenyl)thiophene-2-yl)-1-methylpyridinium trifluoromethanesulfonate

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Chemical Property of 4-(5-(4-(dihexylamino)phenyl)thiophene-2-yl)-1-methylpyridinium trifluoromethanesulfonate

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Technology Process of 4-(5-(4-(dihexylamino)phenyl)thiophene-2-yl)-1-methylpyridinium trifluoromethanesulfonate

There total 5 articles about 4-(5-(4-(dihexylamino)phenyl)thiophene-2-yl)-1-methylpyridinium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1236567-70-6
N,N-dihexyl-4-(5-(pyridin-4-yl)thiophene-2-yl)benzenamine

: 333-27-7
methyl trifluoromethanesulfonate

: 1236567-78-4
4-(5-(4-(dihexylamino)phenyl)thiophene-2-yl)-1-methylpyridinium trifluoromethanesulfonate

Guidance literature:: In dichloromethane; at 0 ℃; for 1h; Cooling with ice;

Reference yield:

: 90134-09-1
N,N-dihexyl-4-iodobenzenamine

: 1236567-78-4
4-(5-(4-(dihexylamino)phenyl)thiophene-2-yl)-1-methylpyridinium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; methanol / 0.5 h / 70 °C / Inert atmosphere

1.2: 9 h / 70 °C / Inert atmosphere

2.1: dichloromethane / 1 h / 0 °C / Cooling with ice

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; dichloromethane; toluene;

Reference yield:

: 638-45-9
1-Iodohexane

: 1236567-78-4
4-(5-(4-(dihexylamino)phenyl)thiophene-2-yl)-1-methylpyridinium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 22 h / 90 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; methanol / 0.5 h / 70 °C / Inert atmosphere

2.2: 9 h / 70 °C / Inert atmosphere

3.1: dichloromethane / 1 h / 0 °C / Cooling with ice

With sodium carbonate; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;