(R)-3-Benzyloxy-tetradecanoic acid [(2R,3R,4R,5S,6R)-2-(4-allyloxy-butoxy)-4,5-dihydroxy-6-trityloxymethyl-tetrahydro-pyran-3-yl]-amide

Base Information

Chemical Name:(R)-3-Benzyloxy-tetradecanoic acid [(2R,3R,4R,5S,6R)-2-(4-allyloxy-butoxy)-4,5-dihydroxy-6-trityloxymethyl-tetrahydro-pyran-3-yl]-amide
CAS No.:155739-45-0
Molecular Formula:C₅₃H₇₁NO₈
Molecular Weight:850.149
Hs Code.:

Synonyms:(R)-3-Benzyloxy-tetradecanoic acid [(2R,3R,4R,5S,6R)-2-(4-allyloxy-butoxy)-4,5-dihydroxy-6-trityloxymethyl-tetrahydro-pyran-3-yl]-amide

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Chemical Property of (R)-3-Benzyloxy-tetradecanoic acid [(2R,3R,4R,5S,6R)-2-(4-allyloxy-butoxy)-4,5-dihydroxy-6-trityloxymethyl-tetrahydro-pyran-3-yl]-amide

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Technology Process of (R)-3-Benzyloxy-tetradecanoic acid [(2R,3R,4R,5S,6R)-2-(4-allyloxy-butoxy)-4,5-dihydroxy-6-trityloxymethyl-tetrahydro-pyran-3-yl]-amide

There total 1 articles about (R)-3-Benzyloxy-tetradecanoic acid [(2R,3R,4R,5S,6R)-2-(4-allyloxy-butoxy)-4,5-dihydroxy-6-trityloxymethyl-tetrahydro-pyran-3-yl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 76-83-5
trityl chloride

: 4-allyloxybutyl 2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-β-D-glucopyranoside

: 155739-45-0
(R)-3-Benzyloxy-tetradecanoic acid [(2R,3R,4R,5S,6R)-2-(4-allyloxy-butoxy)-4,5-dihydroxy-6-trityloxymethyl-tetrahydro-pyran-3-yl]-amide

Guidance literature:: With pyridine; for 24h; Ambient temperature;
DOI:10.1016/0008-6215(94)84290-6

Reference yield: 84.0%

: 87357-67-3
(R)-3-benzyloxytetradecanoic acid

: 155739-45-0
(R)-3-Benzyloxy-tetradecanoic acid [(2R,3R,4R,5S,6R)-2-(4-allyloxy-butoxy)-4,5-dihydroxy-6-trityloxymethyl-tetrahydro-pyran-3-yl]-amide

: 4-allyloxybutyl 2-<(R)-3-benzyloxytetradecanamido>-3,4-di-O-<(R)-3-benzyloxytetradecanoyl>-2-deoxy-6-O-trityl-β-D-glucopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 2.5h;
DOI:10.1016/0008-6215(94)84290-6

Reference yield:

: 87357-76-4
(R)-3-(dodecanoyloxy)tetradecanoic acid

: 155739-45-0
(R)-3-Benzyloxy-tetradecanoic acid [(2R,3R,4R,5S,6R)-2-(4-allyloxy-butoxy)-4,5-dihydroxy-6-trityloxymethyl-tetrahydro-pyran-3-yl]-amide

: (R)-3-Tetradecanoyloxy-tetradecanoic acid (2R,3S,4R,5R,6R)-6-(4-allyloxy-butoxy)-5-((R)-3-benzyloxy-tetradecanoylamino)-4-hydroxy-2-trityloxymethyl-tetrahydro-pyran-3-yl ester

: 155751-71-6
4-allyloxybutyl 2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-3-O-<(R)-3-tetradecanoyloxytetradecanoyl>-6-O-trityl-β-D-glucopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 4h; Yield given. Yields of byproduct given;
DOI:10.1016/0008-6215(94)84290-6