Chloro-acetic acid 4-((E)-2-chlorocarbonyl-vinyl)-2-methoxy-phenyl ester

Base Information

Chemical Name:Chloro-acetic acid 4-((E)-2-chlorocarbonyl-vinyl)-2-methoxy-phenyl ester
CAS No.:190122-90-8
Molecular Formula:C₁₂H₁₀Cl₂O₄
Molecular Weight:289.115
Hs Code.:

Synonyms:Chloro-acetic acid 4-((E)-2-chlorocarbonyl-vinyl)-2-methoxy-phenyl ester

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Chemical Property of Chloro-acetic acid 4-((E)-2-chlorocarbonyl-vinyl)-2-methoxy-phenyl ester

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Technology Process of Chloro-acetic acid 4-((E)-2-chlorocarbonyl-vinyl)-2-methoxy-phenyl ester

There total 2 articles about Chloro-acetic acid 4-((E)-2-chlorocarbonyl-vinyl)-2-methoxy-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 190122-81-7
(E)-3-[4-(2-Chloro-acetoxy)-3-methoxy-phenyl]-acrylic acid

: 190122-90-8
Chloro-acetic acid 4-((E)-2-chlorocarbonyl-vinyl)-2-methoxy-phenyl ester

Guidance literature:: With thionyl chloride; In benzene; for 0.833333h; Heating;
DOI:10.1016/S0008-6215(97)00032-3

Reference yield:

: 1135-24-6,537-98-4
(E)-3-(4-hydroxy-3-methoxyphenyl)acrylic acid

: 190122-90-8
Chloro-acetic acid 4-((E)-2-chlorocarbonyl-vinyl)-2-methoxy-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 75.3 percent / NaOH / methanol / 0.05 h

2: 93 percent / SOCl₂ / benzene / 0.83 h / Heating

With sodium hydroxide; thionyl chloride; In methanol; benzene;
DOI:10.1016/S0008-6215(97)00032-3

Reference yield:

: 190122-90-8
Chloro-acetic acid 4-((E)-2-chlorocarbonyl-vinyl)-2-methoxy-phenyl ester

: 110978-95-5
2-(4-hydroxyphenyl)ethyl 6-O-(E)-(3-methoxy-4-hydroxy)cinnamoyl β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 61.5 percent / CH₂Cl₂; pyridine / 20 h / 10 °C

2: NH₄OAc / methanol / 1 h / Heating

3: 380 mg / PdCl₂, CuCl / methanol / 4 h / 25 °C

With ammonium acetate; copper(l) chloride; palladium dichloride; In pyridine; methanol; dichloromethane;
DOI:10.1016/S0008-6215(97)00032-3