N-benzoylnorthebaine

Base Information

Chemical Name:N-benzoylnorthebaine
CAS No.:110173-63-2
Molecular Formula:C₂₅H₂₃NO₄
Molecular Weight:401.462
Hs Code.:

Synonyms:N-benzoylnorthebaine

Suppliers and Price of N-benzoylnorthebaine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-benzoylnorthebaine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-benzoylnorthebaine

There total 1 articles about N-benzoylnorthebaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 93-97-0
benzoic acid anhydride

: 7679-18-7
N-desmethylthebaine hydrochloride

: 110173-63-2
N-benzoylnorthebaine

Guidance literature:: With triethylamine; In dichloromethane; Ambient temperature;
DOI:10.1021/jm00394a016

Reference yield: 99.0%

: 108-31-6
maleic anhydride

: 110173-63-2
N-benzoylnorthebaine

: 110173-64-3
N-benzoylnorthebaine maleic anhydride adduct

Guidance literature:: In benzene; for 7h; Heating;
DOI:10.1021/jm00394a016

Reference yield:

: 110173-63-2
N-benzoylnorthebaine

: 110173-27-8
N-benzyl-7α-formyl-8α-<<(tert-butyldimethylsilyl)oxy>methyl>-endo-ethylenetetrahydronorthebaine

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / benzene / 7 h / Heating

2: 64 percent / lithium aluminum hydride / tetrahydrofuran / 3 h / Heating

3: 1.) KH, 2.) n-BuLi

4: 99 percent / oxalyl chloride, DMSO / CH₂Cl₂ / 1 h / -78 - -40 °C

With lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; potassium hydride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/jm00394a016