9,9-dimethyl-12-(4-methylphenyl)-8,9,10,12-tetrahydrobenzo[a]xanthene-11-one

Base Information

• Chemical Name: 9,9-dimethyl-12-(4-methylphenyl)-8,9,10,12-tetrahydrobenzo[a]xanthene-11-one
• CAS No.: 1173694-38-6
• Molecular Formula: C₂₆H₂₄O₂
• Molecular Weight: 368.475
• Mol file: 1173694-38-6.mol

Synonyms:9,9-dimethyl-12-(4-methylphenyl)-8,9,10,12-tetrahydrobenzo[a]xanthene-11-one

Chemical Property of 9,9-dimethyl-12-(4-methylphenyl)-8,9,10,12-tetrahydrobenzo[a]xanthene-11-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9,9-dimethyl-12-(4-methylphenyl)-8,9,10,12-tetrahydrobenzo[a]xanthene-11-one

There total 1 articles about 9,9-dimethyl-12-(4-methylphenyl)-8,9,10,12-tetrahydrobenzo[a]xanthene-11-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-methyl-benzaldehyde (104-87-0) + dimedone (126-81-8) + β-naphthol (135-19-3) → 9,9-dimethyl-12-(4-methylphenyl)-8,9,10,12-tetrahydrobenzo[a]xanthene-11-one (1173694-38-6)

Guidance literature:

With 1,3,5-Triazo-2,4,6-triphosphorine-2,2,4,4,6,6-hexachloride supported on boehmite nanoparticles; In neat (no solvent); at 80 ℃; for 0.133333h; Green chemistry;

DOI:10.1039/c4nj01128g

Reference yield: 80.0%

9,9-dimethyl-12-(4-methylphenyl)-8,9,10,12-tetrahydrobenzo[a]xanthene-11-one (1173694-38-6) → 9,9-dimethyl-12-(4-tolyl)-8,9,10,12-tetrahydrobenzo[a]xanthene-11-thione (1416451-18-7)

Guidance literature:

With Lawessons reagent; In toluene; for 0.666667h; Reflux;

DOI:10.1016/j.ejmech.2012.10.025

Reference yield:

9,9-dimethyl-12-(4-methylphenyl)-8,9,10,12-tetrahydrobenzo[a]xanthene-11-one (1173694-38-6) + toluene-4-sulfonic acid hydrazide (1576-35-8) → C33H32N2O3S

Guidance literature:

With hydrogenchloride; In methanol; chloroform; for 3h; Reflux;

DOI:10.1016/j.molstruc.2021.132297

upstream raw materials:

4-methyl-benzaldehyde

dimedone

β-naphthol

Downstream raw materials:

9,9-dimethyl-12-(4-tolyl)-8,9,10,12-tetrahydrobenzo[a]xanthene-11-thione