C₂₆H₁₈⁽²⁾HNO₄

Base Information

Chemical Name:C₂₆H₁₈⁽²⁾HNO₄
CAS No.:1435518-62-9
Molecular Formula:C₂₆H₁₉NO₄
Molecular Weight:410.433
Hs Code.:

C<sub>26</sub>H<sub>18</sub><sup>(2)</sup>HNO<sub>4</sub>

Synonyms:C₂₆H₁₈⁽²⁾HNO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₁₈⁽²⁾HNO₄

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Technology Process of C₂₆H₁₈⁽²⁾HNO₄

There total 8 articles about C₂₆H₁₈⁽²⁾HNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: deuterio-3,7-diphenylhepta-1,6-diyn-3-ol

: 122-04-3
4-nitro-benzoyl chloride

: 1435518-62-9
C₂₆H₁₈⁽²⁾HNO₄

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1021/ja4032727

Reference yield:

: 30780-51-9
5-phenylpent-4-ynoic acid methyl ester

: 1435518-62-9
C₂₆H₁₈⁽²⁾HNO₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hydroxide / 1,4-dioxane; water / 20 °C / Inert atmosphere

2.1: 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 15 h / 20 °C / Inert atmosphere

3.1: tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere

4.2: 3 h / -78 - 20 °C / Inert atmosphere

5.1: potassium carbonate / methanol / 20 °C / Inert atmosphere

6.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

6.2: 0.5 h / 20 °C / Inert atmosphere

7.1: dmap; triethylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; dmap; n-butyllithium; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; potassium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; cyclohexane; water;
DOI:10.1021/ja4032727

Reference yield:

: 3350-92-3
5-phenylpent-4-ynoic acid

: 1435518-62-9
C₂₆H₁₈⁽²⁾HNO₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 15 h / 20 °C / Inert atmosphere

2.1: tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere

3.2: 3 h / -78 - 20 °C / Inert atmosphere

4.1: potassium carbonate / methanol / 20 °C / Inert atmosphere

5.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

5.2: 0.5 h / 20 °C / Inert atmosphere

6.1: dmap; triethylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; dmap; n-butyllithium; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; cyclohexane;
DOI:10.1021/ja4032727